Jurnal
Synthesis and Characterization of 1-(1-naphthyl)-5-phenyl-2,4-pentadien-1-one from trans-cinnamaldehyde and 1-acetonaphthone
al Kimiya: Jurnal Ilmu Kimia dan Terapan
ISSN 2407-1927, 2407-1897
Terbit 2023-06-30
Penerbit Department of Chemistry, Faculty of Science and Technology, UIN Sunan Gunung Djati Bandung
Bahasa eng
Abstrak
Chalcone analogues (1-(1-naphthyl)-5-phenyl-2,4-pentadiene-1-one) have been synthesized through an aldol condensation reaction between cinnamaldehyde and 1-acetylnaphthalene. The method used in this study is the stirrer method, with the reaction conducted at room temperature for 24 hours using a NaOH catalyst in H2O/ethanol (50%, v/v). The purity of the product was analyzed using thin-layer chromatography on silica gel plates with n-hexane: ethyl acetate (9:1) employed as the solvent. The resulting product obtained was 0.88 g with a yield of 61.97%. Structure Analysis and elucidation of the synthesized compounds were performed by measuring the vibrations of the functional groups using FTIR, LCMSMS analysis, and determining the 1H and 13C atoms by HNMR and CNMR analysis. The FTIR, LCMSMS, 1H, and 13C NMR analysis identified that the synthesized product as chalcone analogues, specifically 1-(1-naphthyl)-5-phenyl-2,4-pentadiene-1-one.
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Sumber metadata: OAI-PMH (metadata jurnal) https://journal.uinsgd.ac.id/index.php/ak/oai, pertama di-harvest 7 Nov 2026, terakhir terlihat 8 Nov 2026.
Metadata asli (oai_dc)
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<dc:title xml:lang="en-US">Synthesis and Characterization of 1-(1-naphthyl)-5-phenyl-2,4-pentadien-1-one from trans-cinnamaldehyde and 1-acetonaphthone</dc:title>
<dc:creator>Fitria, Dori</dc:creator>
<dc:creator>Ardiansah, Bayu</dc:creator>
<dc:creator>Balkis, Atia</dc:creator>
<dc:subject xml:lang="en-US">Chalcone analogues</dc:subject>
<dc:subject xml:lang="en-US">aldol condensation reaction</dc:subject>
<dc:subject xml:lang="en-US">cinnamaldehyde</dc:subject>
<dc:subject xml:lang="en-US">1-acetylnaphthalene</dc:subject>
<dc:subject xml:lang="en-US">1-(1-naphthyl)-5-phenyl-2</dc:subject>
<dc:subject xml:lang="en-US">4-pentadiene-1-one</dc:subject>
<dc:description xml:lang="en-US">Chalcone analogues (1-(1-naphthyl)-5-phenyl-2,4-pentadiene-1-one) have been synthesized through an aldol condensation reaction between cinnamaldehyde and 1-acetylnaphthalene. The method used in this study is the stirrer method, with the reaction conducted at room temperature for 24 hours using a NaOH catalyst in H2O/ethanol (50%, v/v). The purity of the product was analyzed using thin-layer chromatography on silica gel plates with n-hexane: ethyl acetate (9:1) employed as the solvent. The resulting product obtained was 0.88 g with a yield of 61.97%. Structure Analysis and elucidation of the synthesized compounds were performed by measuring the vibrations of the functional groups using FTIR, LCMSMS analysis, and determining the 1H and 13C atoms by HNMR and CNMR analysis. The FTIR, LCMSMS, 1H, and 13C NMR analysis identified that the synthesized product as chalcone analogues, specifically 1-(1-naphthyl)-5-phenyl-2,4-pentadiene-1-one.</dc:description>
<dc:publisher xml:lang="en-US">Department of Chemistry, Faculty of Science and Technology, UIN Sunan Gunung Djati Bandung</dc:publisher>
<dc:date>2023-06-30</dc:date>
<dc:type>info:eu-repo/semantics/article</dc:type>
<dc:type>info:eu-repo/semantics/publishedVersion</dc:type>
<dc:format>application/pdf</dc:format>
<dc:format>application/vnd.openxmlformats-officedocument.wordprocessingml.document</dc:format>
<dc:identifier>https://journal.uinsgd.ac.id/index.php/ak/article/view/22896</dc:identifier>
<dc:identifier>10.15575/ak.v10i1.22896</dc:identifier>
<dc:source xml:lang="en-US">al Kimiya: Jurnal Ilmu Kimia dan Terapan; Vol. 10 No. 1 (2023): al Kimiya: Jurnal Ilmu Kimia dan Terapan; 13-19</dc:source>
<dc:source>2407-1927</dc:source>
<dc:source>2407-1897</dc:source>
<dc:source>10.15575/ak.v10i1</dc:source>
<dc:language>eng</dc:language>
<dc:relation>https://journal.uinsgd.ac.id/index.php/ak/article/view/22896/9229</dc:relation>
<dc:relation>https://journal.uinsgd.ac.id/index.php/ak/article/view/22896/13154</dc:relation>
<dc:rights xml:lang="en-US">Copyright (c) 2023 Dori Fitria</dc:rights>
</oai_dc:dc>
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APA 7
Fitria, D., Ardiansah, B., & Balkis, A. (2023). Synthesis and Characterization of 1-(1-naphthyl)-5-phenyl-2,4-pentadien-1-one from trans-cinnamaldehyde and 1-acetonaphthone. al Kimiya: Jurnal Ilmu Kimia dan Terapan, 10(1), 13–19. https://doi.org/10.15575/ak.v10i1.22896
Salin
IEEE
D. Fitria, B. Ardiansah, and A. Balkis, “Synthesis and Characterization of 1-(1-naphthyl)-5-phenyl-2,4-pentadien-1-one from trans-cinnamaldehyde and 1-acetonaphthone,” al Kimiya: Jurnal Ilmu Kimia dan Terapan, vol. 10, no. 1, pp. 13–19, 2023, doi: 10.15575/ak.v10i1.22896.
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