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Effect of Low Solid/Liquid Ratio on Hydrothermal Synthesis of Hydroxyapatite with Green Template from Banana Flower (Musa acuminata Cavendish)

al Kimiya: Jurnal Ilmu Kimia dan Terapan · Vol. 10 No. 1 (2023) · hlm. 57–63

DOI
10.15575/ak.v10i1.25262
ISSN
2407-1927, 2407-1897
Terbit
2023-06-30
Penerbit
Department of Chemistry, Faculty of Science and Technology, UIN Sunan Gunung Djati Bandung
Bahasa
eng

Abstrak

Hydroxyapatite (HA) was successfully synthesized using the hydrothermal method. This study aimed to analyze the effect of a low solid/liquid ratio on the properties of HA crystals. HA synthesis was performed using chicken eggshells and the hydrothermal method at a temperature of 150°C. The solvent amount was kept constant, while the solid amount varied (half-reaction). The characteristics of HA were determined using XRD, FTIR, PSA, and SEM. The results showed that the purity and size of HA were influenced by a low solid/liquid ratio, while the crystallinity remained relatively unchanged, directly impacting the lattice parameter value. FTIR analysis revealed the absence of the O-H group in the sample with the low solid/liquid ratio. PSA results showed a smaller particle size of 0.995 µm for the sample with the low solid/liquid ratio. SEM results demonstrated a smaller particle size in the sample with a low solid/liquid ratio when observed at the same magnification

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  • Sunan Gunung Djati State Islamic University Bandung
  • Padjadjaran University
  • Mulawarman University
  • University of Malaya
  • Universitas Halu Oleo
  • National University of Malaysia
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Rekan penulisOrganisasiArtikel bersama
Vina AmaliaSunan Gunung Djati State Islamic University Bandung5
Dede SuhendarSunan Gunung Djati State Islamic University Bandung4
Yusuf RohmatullohSunan Gunung Djati State Islamic University Bandung2
Mukhamad NurhadiMulawarman University2
Yudha Prawira BudimanPadjadjaran University2
Dyah Dwi PoerwantoSunan Gunung Djati State Islamic University Bandung1
Soehartini IsnainiAfiliasi tidak diketahui1
Yuna WidayantiSunan Gunung Djati State Islamic University Bandung1
Robby'atul Adawiyah HanifahSunan Gunung Djati State Islamic University Bandung1
Gina Giftia Azmiana DelilahSunan Gunung Djati State Islamic University Bandung1
Resi RosantiSunan Gunung Djati State Islamic University Bandung1
Citra Fitiriani KusmanSunan Gunung Djati State Islamic University Bandung1
Ahmad HidayatUniversitas Halu Oleo1
Soni SetiadjiSunan Gunung Djati State Islamic University Bandung1
Kurniawati KurniawatiSunan Gunung Djati State Islamic University Bandung1
Riki JuniansyahSunan Gunung Djati State Islamic University Bandung1
Fatimah LayyinahSunan Gunung Djati State Islamic University Bandung1
Farida ZaharaSunan Gunung Djati State Islamic University Bandung1
Dyanti Nur'aeniSunan Gunung Djati State Islamic University Bandung1
W SumarniSunan Gunung Djati State Islamic University Bandung1
Riska Farah DibaSunan Gunung Djati State Islamic University Bandung1
Ayu Novi RiantySunan Gunung Djati State Islamic University Bandung1
Ratna KusumawardaniMulawarman University1
Akrajas Ali UmarNational University of Malaysia1
Qistholina Dewi KulsumSunan Gunung Djati State Islamic University Bandung1
Sidiq Abdull RoufSunan Gunung Djati State Islamic University Bandung1
Idad SuhadaSunan Gunung Djati State Islamic University Bandung1
Riseu MeisaniSunan Gunung Djati State Islamic University Bandung1
Moch Yogi Santika NugrahaSunan Gunung Djati State Islamic University Bandung1
Narisha ZuhraSunan Gunung Djati State Islamic University Bandung1
Riri AisyahSunan Gunung Djati State Islamic University Bandung1
Neneng WindayaniSunan Gunung Djati State Islamic University Bandung1
Meila N EffendiSunan Gunung Djati State Islamic University Bandung1

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Sumber metadata: OAI-PMH (metadata jurnal) https://journal.uinsgd.ac.id/index.php/ak/oai, pertama di-harvest 7 Nov 2026, terakhir terlihat 8 Nov 2026.
Metadata asli (oai_dc) 
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	<dc:title xml:lang="en-US">Effect of Low Solid/Liquid Ratio on Hydrothermal Synthesis of Hydroxyapatite with Green Template from Banana Flower (Musa acuminata Cavendish)</dc:title>
	<dc:creator>Irwansyah, Ferli Septi</dc:creator>
	<dc:creator>Amal, Alfi Ikhlasul</dc:creator>
	<dc:creator>Hadisantoso, Eko Prabowo</dc:creator>
	<dc:creator>Noviyanti, Atiek Rostika</dc:creator>
	<dc:creator>Eddy, Diana Rakhmawaty</dc:creator>
	<dc:creator>Ma'Amor, Azman Bin</dc:creator>
	<dc:creator>Risdiana, Risdiana</dc:creator>
	<dc:subject xml:lang="en-US">Hydroxyapatite</dc:subject>
	<dc:subject xml:lang="en-US">hydrothermal</dc:subject>
	<dc:subject xml:lang="en-US">solid/liquid ratio</dc:subject>
	<dc:subject xml:lang="en-US">green template</dc:subject>
	<dc:subject xml:lang="en-US">banana flower</dc:subject>
	<dc:description xml:lang="en-US">Hydroxyapatite (HA) was successfully synthesized using the hydrothermal method. This study aimed to analyze the effect of a low solid/liquid ratio on the properties of HA crystals. HA synthesis was performed using chicken eggshells and the hydrothermal method at a temperature of 150°C. The solvent amount was kept constant, while the solid amount varied (half-reaction). The characteristics of HA were determined using XRD, FTIR, PSA, and SEM. The results showed that the purity and size of HA were influenced by a low solid/liquid ratio, while the crystallinity remained relatively unchanged, directly impacting the lattice parameter value. FTIR analysis revealed the absence of the O-H group in the sample with the low solid/liquid ratio. PSA results showed a smaller particle size of 0.995 µm for the sample with the low solid/liquid ratio. SEM results demonstrated a smaller particle size in the sample with a low solid/liquid ratio when observed at the same magnification</dc:description>
	<dc:publisher xml:lang="en-US">Department of Chemistry, Faculty of Science and Technology, UIN Sunan Gunung Djati Bandung</dc:publisher>
	<dc:date>2023-06-30</dc:date>
	<dc:type>info:eu-repo/semantics/article</dc:type>
	<dc:type>info:eu-repo/semantics/publishedVersion</dc:type>
	<dc:format>application/pdf</dc:format>
	<dc:identifier>https://journal.uinsgd.ac.id/index.php/ak/article/view/25262</dc:identifier>
	<dc:identifier>10.15575/ak.v10i1.25262</dc:identifier>
	<dc:source xml:lang="en-US">al Kimiya: Jurnal Ilmu Kimia dan Terapan; Vol. 10 No. 1 (2023): al Kimiya: Jurnal Ilmu Kimia dan Terapan; 57-63</dc:source>
	<dc:source>2407-1927</dc:source>
	<dc:source>2407-1897</dc:source>
	<dc:source>10.15575/ak.v10i1</dc:source>
	<dc:language>eng</dc:language>
	<dc:relation>https://journal.uinsgd.ac.id/index.php/ak/article/view/25262/9234</dc:relation>
	<dc:rights xml:lang="en-US">Copyright (c) 2023 Ferli Septi Irwansyah</dc:rights>
</oai_dc:dc>