Jurnal
Effect of Preparation Acetone on Fish Bones Synthesized Through Sintering Method to Improve Hydroxyapatite Characteristics
al Kimiya: Jurnal Ilmu Kimia dan Terapan · Vol. 10 No. 2 (2023) · hlm. 87–97
- ISSN
- 2407-1927, 2407-1897
- Terbit
- 2023-12-31
- Penerbit
- Department of Chemistry, Faculty of Science and Technology, UIN Sunan Gunung Djati Bandung
- Bahasa
- eng
Abstrak
In the development of advanced materials and various technological applications, the preparation and sintering processes have become two important factors in determining material characteristics. This research focuses on two main aspects, namely the effect of fish bone preparation by soaking in acetone and the surface area of the material in the sintering process as part of the process of developing better materials. This research aims to determine the effect of soaking fish bone powder with acetone and the effect of the surface area of sintered fish bones to produce hydroxyapatite (HA). The immersion process with acetone is included in the sample preparation stage, while the sintering process is included in the material synthesis stage. These two things can affect the characteristics of the HA produced after analysis from the X-ray diffraction test. The HA structure obtained from all samples is hexagonal with cell parameter values a = b ≠c and space group P 63 / m, where all samples have a value range of a = b = 9,42 Å and c = 6,88 Å. HA crystallinity was identified through the XRD peak at 2θ = 25,8 (002); 31,7 (211); 32,1 (112); 32,8 (300); 34,0 (202); 39,7 (310); 46,6 (222); 49,4 (213); 50,4 (321). The PAF-900 and CAF-900 samples are similar to HA in JCPDS 01-089-4405 whose compound formula is Ca5(PO4)3(OH) while the PWAF-900 sample is similar to HA in JCPDS 01-075-3727 whose compound formula is Ca5(PO4)3(CO3)0.01(OH)1.3. The percentage of crystallinity of PAF-900, CAF-900, and PWAF-900 respectively was 84,767; 73,506; and 71,962% with HA grain sizes of 0,8964; 0,6808, and 0,7398 nm. The HA density of PAF-900 and CAF-900 samples is 3,149 g/cm3 while PWAF-900 is 3,146 g/cm3. Based on this description, it can be concluded that the soaking preparation stage with acetone produces HA with the chemical formula Ca5(PO4)3OH with a higher percentage of crystallization and is denser compared to HA obtained without going through the soaking preparation stage with acetone. The sintering stage also plays an important role in increasing the crystallization percentage. The surface area of the material being sintered also influences the percentage of crystallization and the grain size of the resulting HA. Sintered fish bone powder produces a greater percentage of crystallization and grain size than fish bone chunks
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- Mulawarman University
- Xiamen University Malaysia
- Padjadjaran University
- Sunan Gunung Djati State Islamic University Bandung
- Xiamen University
- University of Technology Malaysia
- National University of Malaysia
- Organisasi lain
- Afiliasi tidak diketahui
- Organisasi berbeda
- Organisasi sama
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Tampilkan sebagai tabel
| Rekan penulis | Organisasi | Artikel bersama |
|---|---|---|
| Sin Yuan Lai | Xiamen University Malaysia | 12 |
| Hadi Nur | University of Technology Malaysia | 12 |
| Teguh Wirawan | Mulawarman University | 6 |
| Wirhanuddin Wirhanuddin | Mulawarman University | 5 |
| Yudha Prawira Budiman | Padjadjaran University | 3 |
| Nabila Nur Agusti | Mulawarman University | 3 |
| Sumari Sumari | State University of Malang | 3 |
| Sri Lestari | Mulawarman University | 3 |
| Iis Intan Widiyowati | Mulawarman University | 2 |
| Rahmat Gunawan | Mulawarman University | 2 |
| Anton Prasetyo | Universitas Islam Negeri Maulana Malik Ibrahim | 2 |
| Eko Prabowo Hadisantoso | Sunan Gunung Djati State Islamic University Bandung | 1 |
| Ferli Septi Irwansyah | Sunan Gunung Djati State Islamic University Bandung | 1 |
| Alfi Ikhlasul Amal | Sunan Gunung Djati State Islamic University Bandung | 1 |
| Diana Rakhmawaty Eddy | Padjadjaran University | 1 |
| Azman Ma’amor | University of Malaya | 1 |
| Risdiana Risdiana | Padjadjaran University | 1 |
| Gabrielle Callista Dwi Putri | Afiliasi tidak diketahui | 1 |
| Suryana Suryana | Afiliasi tidak diketahui | 1 |
| Azman Bin Ma’Amor | Afiliasi tidak diketahui | 1 |
| Sheela Chandren | University of Technology Malaysia | 1 |
| Nazarudin Nazarudin | Universitas Jambi | 1 |
| Soerja Koesnarpadi | Mulawarman University | 1 |
| Yuniar Ponco Prananto | University of Brawijaya | 1 |
| Volkan Degirmenci | University of Warwick | 1 |
| Siew Fan Wong | Asia Pacific University of Technology & Innovation | 1 |
| Kelvert Kong | Xiamen University Malaysia | 1 |
| Zhiying Zhu | Xiamen University Malaysia | 1 |
| Lik Quan Lau | Xiamen University Malaysia | 1 |
| Haiyan Li | Xiamen University | 1 |
| Cheng Loong Ngan | Xiamen University | 1 |
| Mahashanon Arumugam | University of Chemistry and Technology, Prague | 1 |
| Lai Sin Yuan | Xiamen University | 1 |
| Muhammad Hatami | Mulawarman University | 1 |
| Chien Yong Goh | Xiamen University Malaysia | 1 |
| Alysa Lau | Xiamen University Malaysia | 1 |
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