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Transesterification of Waste Cooking Oil using CaO Catalyst Derived from Madura Limestone for Biodiesel Production and Its Application in Diesel Engine

Automotive Experiences · Vol. 6 No. 1 (2023) · hlm. 80–93

DOI
10.31603/ae.7879
ISSN
2615-6636, 2615-6202
Terbit
2023-03-19
Penerbit
Universitas Muhammadiyah Magelang
Bahasa
en

Abstrak

In this study, we report biodiesel production from waste cooking oil using CaO catalyst derived from Madura limestone through a transesterification reaction. Many limestone quarries in Madura can be used as heterogeneous catalysts because they are cheap, easy to separate, and have high basicity. Conversion of limestone into CaO catalyst through calcination at 900°C for 3 hours. The CaO catalyst formed was characterized using X-Ray Diffraction (XRD), Fourier Transform Infra-Red (FTIR), and Scanning Electron Microscopy-Energy Dispersive X-Ray (SEM-EDX) instruments. Biodiesel formed through the transesterification reaction was analyzed using GC-MS. Furthermore, biodiesel blends from waste cooking oil and pure diesel were prepared in volume percentages (B-10, B-20, B-30, B-40, and B-100) for testing on diesel engine performance. The results of testing the highest torque and brake horsepower (BHP) were obtained on pure diesel fuel (S-100) at 2.49 Nm and 381.12 watts, respectively. The lowest fuel consumption at 1500 rpm is produced on the B-20 at 0.186 kg/h. Overall, the emission characteristics of carbon monoxide (CO), nitrogen oxides (NOx), and nitrogen monoxide (NO) with the lowest concentration resulted from biodiesel blends rather than pure diesel.

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  • Universiti Teknologi MARA
  • Universitas Bina Sarana Informatika
  • Universitas Halu Oleo
  • National Research and Innovation Agency
  • Institut Agama Islam Negeri Kendari
  • Hasanuddin University
  • Afiliasi tidak diketahui
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Rekan penulisOrganisasiArtikel bersama
Misbakhul FatahAfiliasi tidak diketahui6
Suprapto SupraptoNational Research and Innovation Agency5
Subekti SubektiAfiliasi tidak diketahui4
Hamzah FansuriAfiliasi tidak diketahui4
Syamsul KamriAfiliasi tidak diketahui3
Badrah UyuniAfiliasi tidak diketahui3
Hartati HartatiInstitut Agama Islam Negeri Kendari3
Sugeng TriwahyonoAfiliasi tidak diketahui3
Hasliza BahrujiAfiliasi tidak diketahui3
Mohamed Imran Mohamed AriffUniversiti Teknologi MARA2
Samsiah Binti AhmadUniversiti Teknologi MARA2
Hasnia AramiAfiliasi tidak diketahui2
- HasliantiAfiliasi tidak diketahui2
Hafiz Shuaib FarooqAfiliasi tidak diketahui2
Agus FakhrinaAfiliasi tidak diketahui2
Aishah Abdul JalilAfiliasi tidak diketahui2
Zainab RamliAfiliasi tidak diketahui2
Ratna EdiatiAfiliasi tidak diketahui2
Imam HidayatAfiliasi tidak diketahui2
Agung Wahyudi BiantoroAfiliasi tidak diketahui2
Ridwansyah RidwansyahUniversitas Bina Sarana Informatika1
Muhammad IqbalHasanuddin University1
Henny DestianaUniversitas Bina Sarana Informatika1
Sugiono SugionoUniversitas Bina Sarana Informatika1
Abdul Hadi Abdul HalimAfiliasi tidak diketahui1
Zalikha ZulkifliUniversiti Teknologi MARA1
Khairulliza Ahmad SallehUniversiti Teknologi MARA1
Nur Anim Abdul HalimAfiliasi tidak diketahui1
Masurah MohamadUniversiti Teknologi MARA1
Anis Zafirah AzmiUniversiti Teknologi MARA1
Yusnaini YusnainiUniversitas Halu Oleo1
La SyahrirUniversitas Halu Oleo1
LD Muhammad Yasir HayaAfiliasi tidak diketahui1

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Sumber metadata: OAI-PMH (metadata jurnal) http://journal.unimma.ac.id/index.php/AutomotiveExperiences/oai, pertama di-harvest 8 Nov 2026, terakhir terlihat 8 Nov 2026.
Metadata asli (oai_dc) 
<oai_dc:dc xmlns="http://www.openarchives.org/OAI/2.0/" xmlns:dc="http://purl.org/dc/elements/1.1/" xmlns:oai_dc="http://www.openarchives.org/OAI/2.0/oai_dc/" xmlns:xsi="http://www.w3.org/2001/XMLSchema-instance" xsi:schemaLocation="http://www.openarchives.org/OAI/2.0/oai_dc/  http://www.openarchives.org/OAI/2.0/oai_dc.xsd">
	<dc:title xml:lang="en">Transesterification of Waste Cooking Oil using CaO Catalyst Derived from Madura Limestone for Biodiesel Production and Its Application in Diesel Engine</dc:title>
	<dc:creator xml:lang="en">Hamid, Abdul</dc:creator>
	<dc:creator xml:lang="en">Jakfar, Amin</dc:creator>
	<dc:creator xml:lang="en">Romaniyah, Sirly Bifadilatur</dc:creator>
	<dc:creator xml:lang="en">Febriana, Ike Dayi</dc:creator>
	<dc:creator xml:lang="en">Abdullah, Mohammad</dc:creator>
	<dc:creator xml:lang="en">Rahmawati, Zeni</dc:creator>
	<dc:creator xml:lang="en">Prasetyoko, Didik</dc:creator>
	<dc:subject xml:lang="en">Biodiesel</dc:subject>
	<dc:subject xml:lang="en">Waste cooking oil</dc:subject>
	<dc:subject xml:lang="en">CaO</dc:subject>
	<dc:subject xml:lang="en">Limestone</dc:subject>
	<dc:subject xml:lang="en">Transesterification</dc:subject>
	<dc:subject xml:lang="en">Diesel engine</dc:subject>
	<dc:description xml:lang="en">In this study, we report biodiesel production from waste cooking oil using CaO catalyst derived from Madura limestone through a transesterification reaction. Many limestone quarries in Madura can be used as heterogeneous catalysts because they are cheap, easy to separate, and have high basicity. Conversion of limestone into CaO catalyst through calcination at 900°C for 3 hours. The CaO catalyst formed was characterized using X-Ray Diffraction (XRD), Fourier Transform Infra-Red (FTIR), and Scanning Electron Microscopy-Energy Dispersive X-Ray (SEM-EDX) instruments. Biodiesel formed through the transesterification reaction was analyzed using GC-MS. Furthermore, biodiesel blends from waste cooking oil and pure diesel were prepared in volume percentages (B-10, B-20, B-30, B-40, and B-100) for testing on diesel engine performance. The results of testing the highest torque and brake horsepower (BHP) were obtained on pure diesel fuel (S-100) at 2.49 Nm and 381.12 watts, respectively. The lowest fuel consumption at 1500 rpm is produced on the B-20 at 0.186 kg/h. Overall, the emission characteristics of carbon monoxide (CO), nitrogen oxides (NOx), and nitrogen monoxide (NO) with the lowest concentration resulted from biodiesel blends rather than pure diesel.</dc:description>
	<dc:publisher xml:lang="en">Universitas Muhammadiyah Magelang</dc:publisher>
	<dc:date>2023-03-19</dc:date>
	<dc:type>info:eu-repo/semantics/article</dc:type>
	<dc:type>info:eu-repo/semantics/publishedVersion</dc:type>
	<dc:format>application/pdf</dc:format>
	<dc:identifier>https://journal.unimma.ac.id/AutomotiveExperiences/article/view/7879</dc:identifier>
	<dc:identifier>10.31603/ae.7879</dc:identifier>
	<dc:source xml:lang="en">Automotive Experiences; Vol. 6 No. 1 (2023); 80-93</dc:source>
	<dc:source>2615-6636</dc:source>
	<dc:source>2615-6202</dc:source>
	<dc:language>en</dc:language>
	<dc:relation>https://journal.unimma.ac.id/AutomotiveExperiences/article/view/7879/4096</dc:relation>
	<dc:rights xml:lang="en">Copyright (c) 2023 Abdul Hamid, Amin Jakfar, Sirly Bifadilatur Romaniyah, Ike Dayi Febriana, Mohammad Abdullah, Zeni Rahmawati, Didik Prasetyoko</dc:rights>
</oai_dc:dc>