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The Influence of Metal Loading Amount on Ni/Mesoporous Silica Extracted from Lapindo Mud Templated by CTAB for Conversion of Waste Cooking Oil into Biofuel

Bulletin of Chemical Reaction Engineering & Catalysis · Vol. ume (2021) · hlm. 22–30

DOI
10.9767/bcrec.16.1.9442.22-30
ISSN
1978-2993
Terbit
2021-03-31
Penerbit
Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)
Bahasa
eng
Lisensi
creativecommons.org/licenses/by-sa/4.0

Abstrak

The synthesis and characterization of Ni/mesoporous silica (Ni/MS) catalysts from Lapindo mud with various metal loading for the hydrocracking of waste cooking oil into biofuel has been conducted. The MS was synthesized by the hydrothermal method using CTAB as a template. The nickel-metal of 4, 6, and 8 wt% was loaded into the MS using salt precursors of Ni(NO3)2.6H2O via wet impregnation, produced the Ni(4)/MS, Ni(6)/MS, and Ni(8)/MS catalysts, respectively. The materials produced were then characterized by X-ray Powder Diffraction (XRD), Fourier-Transform Infrared Spectroscopy (FT-IR), and Surface Area Analyzer (SAA), and Absorption Atomic Spectrophotometry (AAS). The catalytic activity test was carried out for hydrocracking of waste cooking oil and the resulted liquid product was analyzed by Gas Chromatography-Mass Spectrometry (GC-MS). The results showed that the specific surface area of Ni(4)/MS, Ni(6)/MS, and Ni(8)/MS catalysts are 63.08, 91.45, and 120.45 m2/g, respectively. The liquid products of the hydrocracking using Ni(4)/MS, Ni(6)/MS, and Ni(8)/MS catalysts were 80.57, 74.63, and 75.77 wt%, where the total biofuel produced was 55.46, 50.93, and 54.05 wt%, respectively. Based on these results, Ni(4)/MS material was successfully used as the most potent catalyst in the hydrocracking of waste cooking oil into the biofuel. Copyright © 2021 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0).

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  • Universitas Gadjah Mada
  • State University of Semarang
  • University of Mataram
  • Hasanuddin University
  • Yogyakarta State University
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TriyonoAfiliasi tidak diketahui6
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Karna WijayaAfiliasi tidak diketahui5
Endah SuarsihAfiliasi tidak diketahui5
Uswatul ChasanahAfiliasi tidak diketahui5
Muhyidin MuhyidinUniversity of Mataram4
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Iman SantosoAfiliasi tidak diketahui3
Nur RahmawatiAfiliasi tidak diketahui2
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Andi Muhammad AnsharHasanuddin University1
S.J, SantosaUniversitas Gadjah Mada1
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Sungkowo Edy MulyonoAfiliasi tidak diketahui1
Woro Apriliana SariAfiliasi tidak diketahui1
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Rama Dirga Dwi SaktiAfiliasi tidak diketahui1
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Endah Fitriani RahayuState University of Semarang1
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Untung RahardjaAfiliasi tidak diketahui1
Wahyu LestariYogyakarta State University1
Sunarto SunartoAfiliasi tidak diketahui1
Dewi SulistianingsihState University of Semarang1
Rahmawati Mohd YusoffAfiliasi tidak diketahui1
Puji Novita SariAfiliasi tidak diketahui1
Sari LestariAfiliasi tidak diketahui1
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Sumber metadata: OAI-PMH (metadata jurnal) https://journal.bcrec.id/index.php/bcrec/oai, pertama di-harvest 8 Nov 2026, terakhir terlihat 8 Nov 2026.
Metadata asli (oai_dc) 
<oai_dc:dc xmlns="http://www.openarchives.org/OAI/2.0/" xmlns:dc="http://purl.org/dc/elements/1.1/" xmlns:oai_dc="http://www.openarchives.org/OAI/2.0/oai_dc/" xmlns:xsi="http://www.w3.org/2001/XMLSchema-instance" xsi:schemaLocation="http://www.openarchives.org/OAI/2.0/oai_dc/  http://www.openarchives.org/OAI/2.0/oai_dc.xsd">
	<dc:title xml:lang="en-US">The Influence of Metal Loading Amount on Ni/Mesoporous Silica Extracted from Lapindo Mud Templated by CTAB for Conversion of Waste Cooking Oil into Biofuel</dc:title>
	<dc:creator>Paramesti, Cahyarani</dc:creator>
	<dc:creator>Trisunaryanti, Wega</dc:creator>
	<dc:creator>Larasati, Savitri</dc:creator>
	<dc:creator>Santoso, Nugroho Raka</dc:creator>
	<dc:creator>Sudiono, Sri</dc:creator>
	<dc:creator>Triyono, Triyono</dc:creator>
	<dc:creator>Fatmawati, Dyah Ayu</dc:creator>
	<dc:subject xml:lang="en-US">Nickel; mesoporous silica; Lapindo mud; CTAB; Waste cooking oil; Biofuel</dc:subject>
	<dc:description xml:lang="en-US">The synthesis and characterization of Ni/mesoporous silica (Ni/MS) catalysts from Lapindo mud with various metal loading for the hydrocracking of waste cooking oil into biofuel has been conducted. The MS was synthesized by the hydrothermal method using CTAB as a template. The nickel-metal of 4, 6, and 8 wt% was loaded into the MS using salt precursors of Ni(NO3)2.6H2O via wet impregnation, produced the Ni(4)/MS, Ni(6)/MS, and Ni(8)/MS catalysts, respectively. The materials produced were then characterized by X-ray Powder Diffraction (XRD), Fourier-Transform Infrared Spectroscopy (FT-IR), and Surface Area Analyzer (SAA), and Absorption Atomic Spectrophotometry (AAS). The catalytic activity test was carried out for hydrocracking of waste cooking oil and the resulted liquid product was analyzed by Gas Chromatography-Mass Spectrometry (GC-MS). The results showed that the specific surface area of Ni(4)/MS, Ni(6)/MS, and Ni(8)/MS catalysts are 63.08, 91.45, and 120.45 m2/g, respectively. The liquid products of the hydrocracking using Ni(4)/MS, Ni(6)/MS, and Ni(8)/MS catalysts were 80.57, 74.63, and 75.77 wt%, where the total biofuel produced was 55.46, 50.93, and 54.05 wt%, respectively. Based on these results, Ni(4)/MS material was successfully used as the most potent catalyst in the hydrocracking of waste cooking oil into the biofuel. Copyright © 2021 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0). </dc:description>
	<dc:publisher xml:lang="en-US">Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)</dc:publisher>
	<dc:date>2021-03-31</dc:date>
	<dc:type>info:eu-repo/semantics/article</dc:type>
	<dc:type>info:eu-repo/semantics/publishedVersion</dc:type>
	<dc:type xml:lang="en-US"></dc:type>
	<dc:format>application/pdf</dc:format>
	<dc:identifier>https://journal.bcrec.id/index.php/bcrec/article/view/9442</dc:identifier>
	<dc:identifier>10.9767/bcrec.16.1.9442.22-30</dc:identifier>
	<dc:source xml:lang="en-US">Bulletin of Chemical Reaction Engineering &amp; Catalysis; 2021: BCREC Volume 16 Issue 1 Year 2021 (March 2021); 22-30</dc:source>
	<dc:source>1978-2993</dc:source>
	<dc:language>eng</dc:language>
	<dc:relation>https://journal.bcrec.id/index.php/bcrec/article/view/9442/5138</dc:relation>
	<dc:rights xml:lang="en-US">Copyright (c) 2021 by Authors, Published by BCREC Group</dc:rights>
	<dc:rights xml:lang="en-US">http://creativecommons.org/licenses/by-sa/4.0</dc:rights>
</oai_dc:dc>