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Hydrazine and Urea Fueled-Solution Combustion Method for Bi2O3 Synthesis: Characterization of Physicochemical Properties and Photocatalytic Activity

Bulletin of Chemical Reaction Engineering & Catalysis · Vol. ume (2020) · hlm. 104–111

DOI
10.9767/bcrec.15.1.5483.104-111
ISSN
1978-2993
Terbit
2020-04-01
Penerbit
Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)
Bahasa
eng
Lisensi
creativecommons.org/licenses/by-sa/4.0

Abstrak

Bismuth oxide synthesis using solution combustion method fuelled by hydrazine and urea has been conducted. This study aims to examine the effect of the applied fuels, urea and hydrazine, on product characteristics and photocatalytic activity in degrading rhodamine B dye. Bismuth oxide synthesis was initiated by dissolving bismuth nitrate pentahydrate (Bi(NO3)3.5H2O) in a nitric acid solvent. Fuel was added and then stirred. The solution formed was heated at 300 ºC for 8 hours. The product obtained was then calcined at 700 ºC for 4 hours. Bismuth oxide synthesized with urea (BO1) and hydrazine (BO2) as fuels both obtained form of yellow powder. The formation of bismuth oxide is indicated by the vibrations of the Bi–O–Bi and Bi–O groups and the crystal structure of a-Bi2O3 in both products. Photocatalytic activity test showed that BO1 has a photocatalyst activity in degrading rhodamine B higher than that of BO2 with constant values of 3.83×10-5 s-1 and 3.43×10-5 s-1, respectively. The high photocatalytic activity can be examined through several factors, such as: band gap values, crystal structure, morphology, and surface area, acquired as a result of the use of different fuels in the synthesis process. Copyright © 2020 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0).

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  • Indonesia University of Education
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  • Badan Pusat Statistik
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Adi DarmawanAfiliasi tidak diketahui4
Arnelli ArnelliAfiliasi tidak diketahui4
Hanaiyah ParasdilaAfiliasi tidak diketahui3
Nurhayati NurhayatiPoliteknik Negeri Ujung Pandang2
Lia HandayaniAfiliasi tidak diketahui2
Risa SuryanaSebelas Maret University2
Siti NurhayatiAfiliasi tidak diketahui2
Pardoyo PardoyoAfiliasi tidak diketahui2
Amilia FauziyahAfiliasi tidak diketahui2
Arum Dista WulansariAfiliasi tidak diketahui2
Rizka AndianingrumAfiliasi tidak diketahui2
Gaurav A. BhaduriAfiliasi tidak diketahui2
Cut RahmawatiAfiliasi tidak diketahui1
Azwar ThaibAfiliasi tidak diketahui1
Agus MuslimBadan Pusat Statistik1
Trie Nanda MulyanaAfiliasi tidak diketahui1
Brainy Happy Ana TasimanAfiliasi tidak diketahui1
Hendri WidyandariAfiliasi tidak diketahui1
Muhammad NashirAfiliasi tidak diketahui1
Khanza Fadhilah AlmasAfiliasi tidak diketahui1
Orien PrilitaAfiliasi tidak diketahui1
Osi ArutantiAfiliasi tidak diketahui1
Agus PurwantoAfiliasi tidak diketahui1
Iqbal FirdausAfiliasi tidak diketahui1
Adama DinaPanuntunAfiliasi tidak diketahui1
Sri HaryantiIndonesia University of Education1
Parsaoran SiahaanIndonesia University of Education1
Agus SubagioAfiliasi tidak diketahui1
Wahyu SetiabudiAfiliasi tidak diketahui1
Heru TjahjanaAfiliasi tidak diketahui1
Marcelinus ChristwardanaDiponegoro University1
Dilla DayantiAfiliasi tidak diketahui1
K. KhoirunnisaAfiliasi tidak diketahui1
H. HadiyantoAfiliasi tidak diketahui1
Achmad Yanuar MaulanaAfiliasi tidak diketahui1

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Sumber metadata: OAI-PMH (metadata jurnal) https://journal.bcrec.id/index.php/bcrec/oai, pertama di-harvest 8 Nov 2026, terakhir terlihat 8 Nov 2026.
Metadata asli (oai_dc) 
<oai_dc:dc xmlns="http://www.openarchives.org/OAI/2.0/" xmlns:dc="http://purl.org/dc/elements/1.1/" xmlns:oai_dc="http://www.openarchives.org/OAI/2.0/oai_dc/" xmlns:xsi="http://www.w3.org/2001/XMLSchema-instance" xsi:schemaLocation="http://www.openarchives.org/OAI/2.0/oai_dc/  http://www.openarchives.org/OAI/2.0/oai_dc.xsd">
	<dc:title xml:lang="en-US">Hydrazine and Urea Fueled-Solution Combustion Method for Bi2O3 Synthesis: Characterization of Physicochemical Properties and Photocatalytic Activity</dc:title>
	<dc:creator>Astuti, Yayuk</dc:creator>
	<dc:creator>Elesta, Prisca Putri</dc:creator>
	<dc:creator>Widodo, Didik Setyo</dc:creator>
	<dc:creator>Widiyandari, Hendri</dc:creator>
	<dc:creator>Balgis, Ratna</dc:creator>
	<dc:subject xml:lang="en-US">Bismuth Oxide; Solution Combustion; Photocatalysis; Rhodamine B, Fuels</dc:subject>
	<dc:description xml:lang="en-US">Bismuth oxide synthesis using solution combustion method fuelled by hydrazine and urea has been conducted. This study aims to examine the effect of the applied fuels, urea and hydrazine, on product characteristics and photocatalytic activity in degrading rhodamine B dye. Bismuth oxide synthesis was initiated by dissolving bismuth nitrate pentahydrate (Bi(NO3)3.5H2O) in a nitric acid solvent. Fuel was added and then stirred. The solution formed was heated at 300 ºC for 8 hours. The product obtained was then calcined at 700 ºC for 4 hours. Bismuth oxide synthesized with urea (BO1) and hydrazine (BO2) as fuels both obtained form of yellow powder. The formation of bismuth oxide is indicated by the vibrations of the Bi–O–Bi and Bi–O groups and the crystal structure of a-Bi2O3 in both products. Photocatalytic activity test showed that BO1 has a photocatalyst activity in degrading rhodamine B higher than that of BO2 with constant values of  3.83×10-5 s-1 and 3.43×10-5 s-1, respectively. The high photocatalytic activity can be examined through several factors, such as: band gap values, crystal structure, morphology, and surface area, acquired as a result of the use of different fuels in the synthesis process. Copyright © 2020 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0).</dc:description>
	<dc:publisher xml:lang="en-US">Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)</dc:publisher>
	<dc:contributor xml:lang="en-US">Ministry of Research, Technology and Higher Education, Republic of Indonesia</dc:contributor>
	<dc:contributor xml:lang="en-US">Diponegoro University</dc:contributor>
	<dc:date>2020-04-01</dc:date>
	<dc:type>info:eu-repo/semantics/article</dc:type>
	<dc:type>info:eu-repo/semantics/publishedVersion</dc:type>
	<dc:type xml:lang="en-US"></dc:type>
	<dc:format>application/pdf</dc:format>
	<dc:identifier>https://journal.bcrec.id/index.php/bcrec/article/view/5483</dc:identifier>
	<dc:identifier>10.9767/bcrec.15.1.5483.104-111</dc:identifier>
	<dc:source xml:lang="en-US">Bulletin of Chemical Reaction Engineering &amp; Catalysis; 2020: BCREC Volume 15 Issue 1 Year 2020 (April 2020); 104-111</dc:source>
	<dc:source>1978-2993</dc:source>
	<dc:language>eng</dc:language>
	<dc:relation>https://journal.bcrec.id/index.php/bcrec/article/view/5483/3419</dc:relation>
	<dc:rights xml:lang="en-US">Copyright (c) 2020 by Authors, Published by BCREC Group</dc:rights>
	<dc:rights xml:lang="en-US">http://creativecommons.org/licenses/by-sa/4.0</dc:rights>
</oai_dc:dc>