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Hydrazine-Fueled Solution Combustion Method: Fuel/Oxidizer Ratio Effects on Photocatalytic Performance of Bismuth Oxide

Bulletin of Chemical Reaction Engineering & Catalysis · Vol. ume (2023) · hlm. 539–547

DOI
10.9767/bcrec.19943
ISSN
1978-2993
Terbit
2023-10-15
Penerbit
Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)
Bahasa
eng
Lisensi
creativecommons.org/licenses/by-sa/4.0

Abstrak

Bismuth oxide nanoparticles were synthesized through the solution combustion method with a variation of fuel: oxidizer (hydrazine: bismuth nitrate) ratios (ϕ) of ϕ 1. Bismuth oxide nanoparticles were characterized by Fourier Transform Infrared Spectroscopy (FTIR), X-Ray Diffraction (XRD), Scanning Electron Microscopy (SEM), and UV-Visible Diffuse Reflectance Spectroscopy (UV-DRS). The FTIR spectra obtained implies that the bismuth oxide nanoparticles of the three ratios contain Bi-O-Bi and Bi-O groups indicating its successful formation. XRD diffractogram suggests that the synthesized bismuth oxide nanoparticles form the α-Bi2O3 crystalline phase for ϕ 1; meanwhile a mixture of α-/β- Bi2O3 phases for ϕ=1. The SEM image illustrates that bismuth oxide nanoparticles form pebble shapes with the ratios in the order of increasing particle sizes of ϕ>1, ϕ=1, and ϕ 1 have respective band gap energies of 2.76 eV, 2.72 eV, and 2.78 eV. The evaluation of the photocatalytic activity of the three bismuth oxide samples shows bismuth oxide with ϕ=1 has the highest photocatalytic activity in remazol black B and methyl orange dyes with rate constants 6.744 x 10-5 s-1 and 7.369 x 10-5 s-1, respectively. Copyright © 2023 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0).

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  • Politeknik Negeri Ujung Pandang
  • Badan Pusat Statistik
  • Diponegoro University
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Rekan penulisOrganisasiArtikel bersama
Nurhayati NurhayatiPoliteknik Negeri Ujung Pandang4
Lia HandayaniAfiliasi tidak diketahui4
Arnelli ArnelliAfiliasi tidak diketahui3
Hendri WidiyandariAfiliasi tidak diketahui2
Cut RahmawatiAfiliasi tidak diketahui2
Azwar ThaibAfiliasi tidak diketahui2
Agus MuslimBadan Pusat Statistik2
Prisca Putri ElestaAfiliasi tidak diketahui1
Didik Setyo WidodoAfiliasi tidak diketahui1
Ratna BalgisAfiliasi tidak diketahui1
Siti NurhayatiAfiliasi tidak diketahui1
Pardoyo PardoyoAfiliasi tidak diketahui1
Amilia FauziyahAfiliasi tidak diketahui1
Arum Dista WulansariAfiliasi tidak diketahui1
Rizka AndianingrumAfiliasi tidak diketahui1
Gaurav A. BhaduriAfiliasi tidak diketahui1
Indriana KartiniAfiliasi tidak diketahui1
Lathifah Puji HastutiAfiliasi tidak diketahui1
Ahmad KusumaatmajaAfiliasi tidak diketahui1
Marcelinus ChristwardanaDiponegoro University1
Dilla DayantiAfiliasi tidak diketahui1
K. KhoirunnisaAfiliasi tidak diketahui1
H. HadiyantoAfiliasi tidak diketahui1
Achmad Yanuar MaulanaAfiliasi tidak diketahui1
Keisya Natania Nur A'intanAfiliasi tidak diketahui1
Iis NurhasanahAfiliasi tidak diketahui1
Fauzan MusthafaAfiliasi tidak diketahui1
Ahmad SusenoAfiliasi tidak diketahui1
Kumala Nadiah SholikaAfiliasi tidak diketahui1
R.A. Yunita Suci RahayuAfiliasi tidak diketahui1
Titik LestariningsihAfiliasi tidak diketahui1
Hasim MuzadiAfiliasi tidak diketahui1
Nayla Zahra KamaliaAfiliasi tidak diketahui1
Muthia ElmaAfiliasi tidak diketahui1
Anna SumardiAfiliasi tidak diketahui1

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Sumber metadata: OAI-PMH (metadata jurnal) https://journal.bcrec.id/index.php/bcrec/oai, pertama di-harvest 8 Nov 2026, terakhir terlihat 8 Nov 2026.
Metadata asli (oai_dc) 
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	<dc:title xml:lang="en-US">Hydrazine-Fueled Solution Combustion Method: Fuel/Oxidizer Ratio Effects on Photocatalytic Performance of Bismuth Oxide</dc:title>
	<dc:creator>Astuti, Yayuk</dc:creator>
	<dc:creator>Mulyana, Trie Nanda</dc:creator>
	<dc:creator>Tasiman, Brainy Happy Ana</dc:creator>
	<dc:creator>Darmawan, Adi</dc:creator>
	<dc:creator>Widyandari, Hendri</dc:creator>
	<dc:subject xml:lang="en-US">Bismuth oxide; Solution Combustion; Fuel-oxidizer ratio; Photocatalyst</dc:subject>
	<dc:description xml:lang="en-US">Bismuth oxide nanoparticles were synthesized through the solution combustion method with a variation of fuel: oxidizer (hydrazine: bismuth nitrate) ratios (ϕ) of ϕ&lt;1, ϕ=1 (stoichiometrically balanced) and ϕ&gt; 1. Bismuth oxide nanoparticles were characterized by Fourier Transform Infrared Spectroscopy (FTIR), X-Ray Diffraction (XRD), Scanning Electron Microscopy (SEM), and UV-Visible Diffuse Reflectance Spectroscopy (UV-DRS). The FTIR spectra obtained implies that the bismuth oxide nanoparticles of the three ratios contain Bi-O-Bi and Bi-O groups indicating its successful formation. XRD diffractogram suggests that the synthesized bismuth oxide nanoparticles form the α-Bi2O3 crystalline phase for ϕ&lt;1 and ϕ&gt;1; meanwhile a mixture of α-/β- Bi2O3 phases for ϕ=1. The SEM image illustrates that bismuth oxide nanoparticles form pebble shapes with the ratios in the order of increasing particle sizes of ϕ&gt;1, ϕ=1, and ϕ&lt;1. The UV-DRS results show that the bismuth oxide with ϕ&lt;1, ϕ=1, and ϕ&gt;1 have respective band gap energies of 2.76 eV, 2.72 eV, and 2.78 eV. The evaluation of the photocatalytic activity of the three bismuth oxide samples shows bismuth oxide with ϕ=1 has the highest photocatalytic activity in remazol black B and methyl orange dyes with rate constants 6.744 x 10-5 s-1 and 7.369 x 10-5 s-1, respectively. Copyright © 2023 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0). </dc:description>
	<dc:publisher xml:lang="en-US">Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)</dc:publisher>
	<dc:date>2023-10-15</dc:date>
	<dc:type>info:eu-repo/semantics/article</dc:type>
	<dc:type>info:eu-repo/semantics/publishedVersion</dc:type>
	<dc:type xml:lang="en-US"></dc:type>
	<dc:format>application/pdf</dc:format>
	<dc:identifier>https://journal.bcrec.id/index.php/bcrec/article/view/19943</dc:identifier>
	<dc:identifier>10.9767/bcrec.19943</dc:identifier>
	<dc:source xml:lang="en-US">Bulletin of Chemical Reaction Engineering &amp; Catalysis; 2023: BCREC Volume 18 Issue 3 Year 2023 (October 2023); 539-547</dc:source>
	<dc:source>1978-2993</dc:source>
	<dc:language>eng</dc:language>
	<dc:relation>https://journal.bcrec.id/index.php/bcrec/article/view/19943/9646</dc:relation>
	<dc:rights xml:lang="en-US">Copyright (c) 2023 by Authors, Published by BCREC Group</dc:rights>
	<dc:rights xml:lang="en-US">https://creativecommons.org/licenses/by-sa/4.0</dc:rights>
</oai_dc:dc>