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Statistical Optimisation using Taguchi Method for Transesterification of Reutealis Trisperma Oil to Biodiesel on CaO-ZnO Catalysts

Bulletin of Chemical Reaction Engineering & Catalysis · Vol. ume (2021) · hlm. 686–695

DOI
10.9767/bcrec.16.3.10648.686-695
ISSN
1978-2993
Terbit
2021-09-30
Penerbit
Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)
Bahasa
eng
Lisensi
creativecommons.org/licenses/by-sa/4.0

Abstrak

Optimisation of biodiesel production from non-edible Reutealis Trisperma oil (RTO) was investigated using Taguchi method. Biodiesel was produced via consecutive esterification and transesterification reactions. Esterification of RTO was carried out using acid catalyst to decrease the amount of free fatty acid from 2.24% to 0.09%. Subsequent transesterification of the treated oil with methanol over a series of CaO-ZnO catalysts was optimized based on the L9 Taguchi orthogonal approach. The optimization parameters are Ca/Zn ratio (0.25, 0.5, and 1), methanol/oil ratio (10, 20, and 30) and reaction time (0.5, 1, and 2 h). CaO-ZnO catalysts at variation of Ca/Zn ratios were prepared using co-precipitation method and characterized using XRD, SEM, TEM, and FTIR analysis. The amount of methyl ester yield was used as the response parameter in the S/N ratio analysis and Analysis of Variance (ANOVA). The optimum parameter for RTO transesterification to biodiesel was determined at Ca/Zn ratio of 1, methanol oil ratio of 30 and reaction time for 2 h. Transesterification under these optimized parameter generated 98% of biodiesel yield, inferring the validity of the statistical approach. Furthermore, ANOVA analysis also confirmed that all the parameters were significantly contributed at approximately equal percentage towards the amount of biodiesel. Copyright © 2021 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0).

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  • Institut Teknologi Sepuluh Nopember
  • Politeknik Negeri Madura
  • Universitas Airlangga
  • University of Technology Malaysia
  • Sebelas Maret University
  • Centre for Advanced Material and Energy Sciences
  • Universiti Brunei Darussalam
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Tampilkan sebagai tabel
Rekan penulisOrganisasiArtikel bersama
Suprapto SupraptoInstitut Teknologi Sepuluh Nopember5
Sugeng TriwahyonoUniversity of Technology Malaysia4
Hamzah FansuriInstitut Teknologi Sepuluh Nopember4
Hartati HartatiUniversitas Airlangga3
Abdul HamidPoliteknik Negeri Madura3
Aishah Abdul JalilUniversity of Technology Malaysia3
Maria UlfaSebelas Maret University3
Abdul Hanif MahadiCentre for Advanced Material and Energy Sciences2
Desy Tri KusumaningtyasInstitut Teknologi Sepuluh Nopember2
Zainab RamliUniversity of Technology Malaysia2
Ratna EdiatiInstitut Teknologi Sepuluh Nopember2
Ike Dayi FebrianaPoliteknik Negeri Madura2
Tri WahyuniInstitut Teknologi Sepuluh Nopember2
Imroatul QoniahInstitut Teknologi Sepuluh Nopember2
Ahmad Anwarud DawamInstitut Teknologi Sepuluh Nopember2
S P RahayuAfiliasi tidak diketahui1
Abdullah EmbongInstitut Teknologi Sepuluh Nopember1
Jasni Mohammad ZainAfiliasi tidak diketahui1
Diah Puspito WulandariInstitut Teknologi Sepuluh Nopember1
Arief KurniawanInstitut Teknologi Sepuluh Nopember1
Alvin NathanaelInstitut Teknologi Sepuluh Nopember1
Anda L. JunianiPoliteknik Perkapalan Negeri Surabaya1
Wardah Rahmatul IslamiyahUniversitas Airlangga1
Abdul Malik BalamiInstitut Teknologi Sepuluh Nopember1
Bambang Widjanarko OtokInstitut Teknologi Sepuluh Nopember1
Mohammad AbdullahUniversiti Teknologi MARA1
Amin JakfarPoliteknik Negeri Madura1
Sirly Bifadilatur RomaniyahPoliteknik Negeri Madura1
Zeni RahmawatiInstitut Teknologi Sepuluh Nopember1
Athirah AyubCentre for Advanced Material and Energy Sciences1
Alfa Akustia WidatiUniversitas Airlangga1
Tanti Kartika DewiUniversitas Airlangga1
Mardi SantosoInstitut Teknologi Sepuluh Nopember1
Yuvita Eka PertiwiSebelas Maret University1

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Sumber metadata: OAI-PMH (metadata jurnal) https://journal.bcrec.id/index.php/bcrec/oai, pertama di-harvest 8 Nov 2026, terakhir terlihat 8 Nov 2026.
Metadata asli (oai_dc) 
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	<dc:title xml:lang="en-US">Statistical Optimisation using Taguchi Method for Transesterification of Reutealis Trisperma Oil to Biodiesel on CaO-ZnO Catalysts</dc:title>
	<dc:creator>Rahmawati, Zeni</dc:creator>
	<dc:creator>Holilah, H.</dc:creator>
	<dc:creator>Purnami, Santi Wulan</dc:creator>
	<dc:creator>Bahruji, Hasliza</dc:creator>
	<dc:creator>Oetami, Titie Prapti</dc:creator>
	<dc:creator>Prasetyoko, Didik</dc:creator>
	<dc:subject xml:lang="en-US">Biodiesel; Reutealis trisperma oil; Taguchi; optimization; Transesterification</dc:subject>
	<dc:description xml:lang="en-US">Optimisation of biodiesel production from non-edible Reutealis Trisperma oil (RTO) was investigated using Taguchi method. Biodiesel was produced via consecutive esterification and transesterification reactions. Esterification of RTO was carried out using acid catalyst to decrease the amount of free fatty acid from 2.24% to 0.09%. Subsequent transesterification of the treated oil with methanol over a series of CaO-ZnO catalysts was optimized based on the L9 Taguchi orthogonal approach. The optimization parameters are Ca/Zn ratio (0.25, 0.5, and 1), methanol/oil ratio (10, 20, and 30) and reaction time (0.5, 1, and 2 h). CaO-ZnO catalysts at variation of Ca/Zn ratios were prepared using co-precipitation method and characterized using XRD, SEM, TEM, and FTIR analysis. The amount of methyl ester yield was used as the response parameter in the S/N ratio analysis and Analysis of Variance (ANOVA). The optimum parameter for RTO transesterification to biodiesel was determined at Ca/Zn ratio of 1, methanol oil ratio of 30 and reaction time for 2 h. Transesterification under these optimized parameter generated 98% of biodiesel yield, inferring the validity of the statistical approach. Furthermore, ANOVA analysis also confirmed that all the parameters were significantly contributed at approximately equal percentage towards the amount of biodiesel. Copyright © 2021 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0). </dc:description>
	<dc:publisher xml:lang="en-US">Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)</dc:publisher>
	<dc:date>2021-09-30</dc:date>
	<dc:type>info:eu-repo/semantics/article</dc:type>
	<dc:type>info:eu-repo/semantics/publishedVersion</dc:type>
	<dc:type xml:lang="en-US"></dc:type>
	<dc:format>application/pdf</dc:format>
	<dc:identifier>https://journal.bcrec.id/index.php/bcrec/article/view/10648</dc:identifier>
	<dc:identifier>10.9767/bcrec.16.3.10648.686-695</dc:identifier>
	<dc:source xml:lang="en-US">Bulletin of Chemical Reaction Engineering &amp; Catalysis; 2021: BCREC Volume 16 Issue 3 Year 2021 (September 2021); 686-695</dc:source>
	<dc:source>1978-2993</dc:source>
	<dc:language>eng</dc:language>
	<dc:relation>https://journal.bcrec.id/index.php/bcrec/article/view/10648/6049</dc:relation>
	<dc:rights xml:lang="en-US">Copyright (c) 2021 by Authors, Published by BCREC Group</dc:rights>
	<dc:rights xml:lang="en-US">https://creativecommons.org/licenses/by-sa/4.0</dc:rights>
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