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Synthesis of Solid Acid Catalyst from Fly Ash for Eugenol Esterification

Bulletin of Chemical Reaction Engineering & Catalysis · Vol. ume (2019) · hlm. 683–688

DOI
10.9767/bcrec.14.3.4254.683-688
ISSN
1978-2993
Terbit
2019-12-01
Penerbit
Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)
Bahasa
eng
Lisensi
creativecommons.org/licenses/by-sa/4.0

Abstrak

A series of fly ash-based heterogeneous acid catalysts were prepared by chemical and thermal treatment. Fly ash was chemically activated using sulfuric acid and followed by thermal activation. Characterization methods of XRD, BET, SEM-EDX, and the performance in esterification of eugenyl acetate production was carried out to reveal the physical and chemical characteristics of prepared catalysts. Activated catalyst showed high silica content (96.5%) and high BET surface area of 70 m2.g-1. The catalyst was proven to be highly active solid acid catalyst for liquid phase esterification of eugenol with acetic acid yielding eugenyl acetate. A yield of 43-48% was obtained with activated fly ash catalysts for 90 minutes reaction. These catalysts may replace beneficially the conventional homogenous liquid acid to the eco-friendly heterogeneous one.

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  • Muhammadiyah University of Surakarta
  • Diponegoro University
  • Universitas Setia Budi
  • Newcastle University
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Rekan penulisOrganisasiArtikel bersama
Indra Viki HartokoMuhammadiyah University of Surakarta2
Muhammad MujiburohmanMuhammadiyah University of Surakarta2
Wahib KhoiruddinMuhammadiyah University of Surakarta2
Marwan EffendyMuhammadiyah University of Surakarta2
Rosi WulandariUniversitas Setia Budi1
Titiek Puji AstutiUniversitas Setia Budi1
Diah AyuMuhammadiyah University of Surakarta1
Rizca AulyanaMuhammadiyah University of Surakarta1
Esti Widya AstutiMuhammadiyah University of Surakarta1
Kusmiyati KusmiyatiMuhammadiyah University of Surakarta1
Didi Dwi AnggoroDiponegoro University1
Luqman BuchoriDiponegoro University1
Yayuk MundriyastutikDiponegoro University1
Keith ScottNewcastle University1

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Sumber metadata: OAI-PMH (metadata jurnal) https://journal.bcrec.id/index.php/bcrec/oai, pertama di-harvest 8 Nov 2026, terakhir terlihat 8 Nov 2026.
Metadata asli (oai_dc) 
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	<dc:title xml:lang="en-US">Synthesis of Solid Acid Catalyst from Fly Ash for Eugenol Esterification</dc:title>
	<dc:creator>Hidayati, Nur</dc:creator>
	<dc:creator>Pujiati, Titik</dc:creator>
	<dc:creator>Prihandini, Elfrida B.</dc:creator>
	<dc:creator>Purnama, Herry</dc:creator>
	<dc:subject xml:lang="en-US">fly ash; solid acid catalyst; esterification; eugenyl acetate</dc:subject>
	<dc:description xml:lang="en-US">A series of fly ash-based heterogeneous acid catalysts were prepared by chemical and thermal treatment. Fly ash was chemically activated using sulfuric acid and followed by thermal activation. Characterization methods of XRD, BET, SEM-EDX, and the performance in esterification of eugenyl acetate production was carried out to reveal the physical and chemical characteristics of prepared catalysts. Activated catalyst showed high silica content (96.5%) and high BET surface area of 70 m2.g-1. The catalyst was proven to be highly active solid acid catalyst for liquid phase esterification of eugenol with acetic acid yielding eugenyl acetate. A yield of 43-48% was obtained with activated fly ash catalysts for 90 minutes reaction. These catalysts may replace beneficially the conventional homogenous liquid acid to the eco-friendly heterogeneous one. </dc:description>
	<dc:publisher xml:lang="en-US">Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)</dc:publisher>
	<dc:contributor xml:lang="en-US"></dc:contributor>
	<dc:date>2019-12-01</dc:date>
	<dc:type>info:eu-repo/semantics/article</dc:type>
	<dc:type>info:eu-repo/semantics/publishedVersion</dc:type>
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	<dc:format>application/pdf</dc:format>
	<dc:identifier>https://journal.bcrec.id/index.php/bcrec/article/view/4254</dc:identifier>
	<dc:identifier>10.9767/bcrec.14.3.4254.683-688</dc:identifier>
	<dc:source xml:lang="en-US">Bulletin of Chemical Reaction Engineering &amp; Catalysis; 2019: BCREC Volume 14 Issue 3 Year 2019 (December 2019); 683-688</dc:source>
	<dc:source>1978-2993</dc:source>
	<dc:language>eng</dc:language>
	<dc:relation>https://journal.bcrec.id/index.php/bcrec/article/view/4254/2672</dc:relation>
	<dc:relation>https://journal.bcrec.id/index.php/bcrec/article/downloadSuppFile/4254/972</dc:relation>
	<dc:relation>https://journal.bcrec.id/index.php/bcrec/article/downloadSuppFile/4254/973</dc:relation>
	<dc:relation>https://journal.bcrec.id/index.php/bcrec/article/downloadSuppFile/4254/974</dc:relation>
	<dc:rights xml:lang="en-US">Copyright (c) 2019 by Authors, Published by BCREC Group</dc:rights>
	<dc:rights xml:lang="en-US">http://creativecommons.org/licenses/by-sa/4.0</dc:rights>
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