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Green Synthesis of Cr-PTC-HIna Metal Organic Frameworks (MOFs) and Its Application in Methylene Blue Photocatalytic Degradation

Bulletin of Chemical Reaction Engineering & Catalysis · Vol. ume (2023) · hlm. 362–374

DOI
10.9767/bcrec.18885
ISSN
1978-2993
Terbit
2023-10-15
Penerbit
Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)
Bahasa
eng
Lisensi
creativecommons.org/licenses/by-sa/4.0

Abstrak

Metal Organic Framework (MOF) is a material that serves as a photocatalyst for decomposing methylene blue pollutant. MOF can be constructed using several kinds of synthetic methods. This study aims to determine the alternative efficient and eco-friendly synthesis method of isonicotinic acid-modulated chromium perylene 3,4,9,10-tetracharboxylate MOF (Cr-PTC-HIna) using solvothermal, hydrothermal, sonochemical, and mechanochemical methods. FTIR analysis revealed that Cr-PTC-HIna was successfully fabricated only by solvothermal, hydrothermal, and sonochemical methods, yielding 40.68%, 44.27%, and 46.50%. Cr-PTC-HIna-ST, Cr-PTC-HIna-HT, and Cr-PTC-HIna-SC have band gap energies of 2.02, 2.02, and 1.98 eV, respectively. Cr-PTC-HIna-HT and Cr-PTC-HIna-SC with irregular shapes form agglomerations. Cr-PTC-HIna-SC had the highest surface area, pore volume, and pore size of 92.76 m2.g−1, 0.3947cm3.g−1, and 142.74 nm, respectively. Cr-PTC-HIna-SC has the highest percentage of methylene blue decolorization through adsorption of 61.843% and photocatalytic degradation of 25.635%. Sonochemical and hydrothermal showed potential as more eco-friendly methods than solvothermal in synthesizing Cr-PTC-HIna MOF. Copyright © 2023 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0).

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  • Syarif Hidayatullah State Islamic University Jakarta
  • Universitas Hasyim Asy'ari
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Siti NurbaytiAfiliasi tidak diketahui19
Nanda SaridewiAfiliasi tidak diketahui18
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Lisa AdhaniAfiliasi tidak diketahui5
Muhammad Shofyan GunawanAfiliasi tidak diketahui5
Sri KomalaAfiliasi tidak diketahui5
Nurhasni NurhasniSyarif Hidayatullah State Islamic University Jakarta5
Adid Adep DwiatmokoAfiliasi tidak diketahui4
Yulyani Nur AzizahAfiliasi tidak diketahui4
Wulandari OktaviaAfiliasi tidak diketahui4
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Farhah Syahidatul MalaAfiliasi tidak diketahui2
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Anna MuawanahSyarif Hidayatullah State Islamic University Jakarta2
Lailatul BadriyahAfiliasi tidak diketahui1
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Novia Dwi RahmawatiUniversitas Hasyim Asy'ari1
Najiah Sephia MaharaniAfiliasi tidak diketahui1

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Sumber metadata: OAI-PMH (metadata jurnal) https://journal.bcrec.id/index.php/bcrec/oai, pertama di-harvest 8 Nov 2026, terakhir terlihat 8 Nov 2026.
Metadata asli (oai_dc) 
<oai_dc:dc xmlns="http://www.openarchives.org/OAI/2.0/" xmlns:dc="http://purl.org/dc/elements/1.1/" xmlns:oai_dc="http://www.openarchives.org/OAI/2.0/oai_dc/" xmlns:xsi="http://www.w3.org/2001/XMLSchema-instance" xsi:schemaLocation="http://www.openarchives.org/OAI/2.0/oai_dc/  http://www.openarchives.org/OAI/2.0/oai_dc.xsd">
	<dc:title xml:lang="en-US">Green Synthesis of Cr-PTC-HIna Metal Organic Frameworks (MOFs) and Its Application in Methylene Blue Photocatalytic Degradation</dc:title>
	<dc:creator>Mahrunnisa, Nur</dc:creator>
	<dc:creator>Adawiah, Adawiah</dc:creator>
	<dc:creator>Aziz, Isalmi</dc:creator>
	<dc:creator>Zulys, Agustino</dc:creator>
	<dc:subject xml:lang="en-US">Hydrothermal; mechanochemical; MOF Cr-PTC-HIna; solvothermal; sonochemical</dc:subject>
	<dc:description xml:lang="en-US">Metal Organic Framework (MOF) is a material that serves as a photocatalyst for decomposing methylene blue pollutant. MOF can be constructed using several kinds of synthetic methods. This study aims to determine the alternative efficient and eco-friendly synthesis method of isonicotinic acid-modulated chromium perylene 3,4,9,10-tetracharboxylate MOF (Cr-PTC-HIna) using solvothermal, hydrothermal, sonochemical, and mechanochemical methods. FTIR analysis revealed that Cr-PTC-HIna was successfully fabricated only by solvothermal, hydrothermal, and sonochemical methods, yielding 40.68%, 44.27%, and 46.50%. Cr-PTC-HIna-ST, Cr-PTC-HIna-HT, and Cr-PTC-HIna-SC have band gap energies of 2.02, 2.02, and 1.98 eV, respectively. Cr-PTC-HIna-HT and Cr-PTC-HIna-SC with irregular shapes form agglomerations. Cr-PTC-HIna-SC had the highest surface area, pore volume, and pore size of 92.76 m2.g−1, 0.3947cm3.g−1, and 142.74 nm, respectively. Cr-PTC-HIna-SC has the highest percentage of methylene blue decolorization through adsorption of 61.843% and photocatalytic degradation of 25.635%. Sonochemical and hydrothermal showed potential as more eco-friendly methods than solvothermal in synthesizing Cr-PTC-HIna MOF. Copyright © 2023 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0). </dc:description>
	<dc:publisher xml:lang="en-US">Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)</dc:publisher>
	<dc:date>2023-10-15</dc:date>
	<dc:type>info:eu-repo/semantics/article</dc:type>
	<dc:type>info:eu-repo/semantics/publishedVersion</dc:type>
	<dc:type xml:lang="en-US"></dc:type>
	<dc:format>application/pdf</dc:format>
	<dc:identifier>https://journal.bcrec.id/index.php/bcrec/article/view/18885</dc:identifier>
	<dc:identifier>10.9767/bcrec.18885</dc:identifier>
	<dc:source xml:lang="en-US">Bulletin of Chemical Reaction Engineering &amp; Catalysis; 2023: BCREC Volume 18 Issue 3 Year 2023 (October 2023); 362-374</dc:source>
	<dc:source>1978-2993</dc:source>
	<dc:language>eng</dc:language>
	<dc:relation>https://journal.bcrec.id/index.php/bcrec/article/view/18885/9611</dc:relation>
	<dc:rights xml:lang="en-US">Copyright (c) 2023 by Authors, Published by BCREC Group</dc:rights>
	<dc:rights xml:lang="en-US">https://creativecommons.org/licenses/by-sa/4.0</dc:rights>
</oai_dc:dc>