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The Effect of Mesoporous H-ZSM-5 Crystallinity as a CaO Support on the Transesterification of Used Cooking Oil

Bulletin of Chemical Reaction Engineering & Catalysis · Vol. ume (2017) · hlm. 329–336

DOI
10.9767/bcrec.12.3.802.329-336
ISSN
1978-2993
Terbit
2017-12-01
Penerbit
Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)
Bahasa
eng
Lisensi
creativecommons.org/licenses/by-sa/4.0

Abstrak

Transesterification of used cooking oil was carried out over calcium oxide supported on mesoporous H-ZSM-5 prepared from kaolin as solid base catalysts. Solid basic catalysts investigated in this study were characterized by XRD, FTIR spectroscopy, and N2 adsorption-desorption techniques. The XRD pattern showed peaks corresponding to the CaO and mesoporous ZSM-5 in the sample. The peak intensity of the CaO increased as CaO loading in ZSM-5 was increased. The characterization based on FTIR spectroscopy revealed that CaO/H-ZSM-5 solids have functional groups characteristics of both CaO and mesoporous H-ZSM-5 which appeared in the band at around 550 cm-1 and 480 cm-1. The isotherm of N2 adsorption-desorption of CaO/H-ZSM-5 indicated the type IV isotherm with the presence of hysteresis loop. For the catalytic activity, the biodiesel yield using catalyst of 10 % CaO/HZSM-5 (100 %), 30 % CaO/HZSM-5 (100 %), 50 % CaO/HZSM-5 (100 %) were 24.34, 27.37, and 29.73 %, respectively. It also related with the basic active site, when loading CaO increased, the basic active site also increased.

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  • Universitas Bina Sarana Informatika
  • National Research and Innovation Agency
  • Institut Agama Islam Negeri Kendari
  • University of Mataram
  • Hasanuddin University
  • Universitas Negeri Surabaya
  • Universitas Halu Oleo
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Rekan penulisOrganisasiArtikel bersama
Zeni RahmawatiAfiliasi tidak diketahui5
Sugeng TriwahyonoAfiliasi tidak diketahui5
Subekti SubektiAfiliasi tidak diketahui4
Aishah Abdul JalilAfiliasi tidak diketahui4
Syamsul KamriAfiliasi tidak diketahui3
Badrah UyuniAfiliasi tidak diketahui3
Hartati HartatiInstitut Agama Islam Negeri Kendari3
Hamzah FansuriAfiliasi tidak diketahui3
Amin JakfarAfiliasi tidak diketahui3
Ike Dayi FebrianaAfiliasi tidak diketahui3
Hasliza BahrujiAfiliasi tidak diketahui3
Hasnia AramiAfiliasi tidak diketahui2
- HasliantiAfiliasi tidak diketahui2
Hafiz Shuaib FarooqAfiliasi tidak diketahui2
Zulkarnain ZulkarnainUniversity of Mataram2
Agus FakhrinaAfiliasi tidak diketahui2
Muslikhin MuslikhinAfiliasi tidak diketahui2
Trimaya Cahya MulatAfiliasi tidak diketahui2
Misbakhul FatahAfiliasi tidak diketahui2
Mahfud MahfudAfiliasi tidak diketahui2
Zainab RamliAfiliasi tidak diketahui2
Ratna EdiatiAfiliasi tidak diketahui2
Imam HidayatAfiliasi tidak diketahui2
Agung Wahyudi BiantoroAfiliasi tidak diketahui2
Ridwansyah RidwansyahUniversitas Bina Sarana Informatika1
Muhammad IqbalHasanuddin University1
Henny DestianaUniversitas Bina Sarana Informatika1
Sugiono SugionoUniversitas Bina Sarana Informatika1
Yurizka Melia SariUniversitas Negeri Surabaya1
Janu ArlinwibowoNational Research and Innovation Agency1
Gupita Nadindra FatimaAfiliasi tidak diketahui1
Dwi PurwokoNational Research and Innovation Agency1
La SyahrirUniversitas Halu Oleo1
LD Muhammad Yasir HayaAfiliasi tidak diketahui1

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Sumber metadata: OAI-PMH (metadata jurnal) https://journal.bcrec.id/index.php/bcrec/oai, pertama di-harvest 8 Nov 2026, terakhir terlihat 8 Nov 2026.
Metadata asli (oai_dc) 
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	<dc:title xml:lang="en-US">The Effect of Mesoporous H-ZSM-5 Crystallinity as a CaO Support on the Transesterification of Used Cooking Oil</dc:title>
	<dc:creator>Purnamasari, Amalia Putri</dc:creator>
	<dc:creator>Sari, Meyga E. F.</dc:creator>
	<dc:creator>Kusumaningtyas, Desy T.</dc:creator>
	<dc:creator>Suprapto, Suprapto</dc:creator>
	<dc:creator>Hamid, Abdul</dc:creator>
	<dc:creator>Prasetyoko, Didik</dc:creator>
	<dc:subject xml:lang="en-US">CaO/H-ZSM-5; Zeolite; Mesoporous; Cooking Oil; Transesterification</dc:subject>
	<dc:description xml:lang="en-US">Transesterification of used cooking oil was carried out over calcium oxide supported on mesoporous H-ZSM-5 prepared from kaolin as solid base catalysts. Solid basic catalysts investigated in this study were characterized by XRD, FTIR spectroscopy, and N2 adsorption-desorption techniques. The XRD pattern showed peaks corresponding to the CaO and mesoporous ZSM-5 in the sample. The peak intensity of the CaO increased as CaO loading in ZSM-5 was increased. The characterization based on FTIR spectroscopy revealed that CaO/H-ZSM-5 solids have functional groups characteristics of both CaO and mesoporous H-ZSM-5 which appeared in the band at around  550 cm-1 and 480 cm-1. The isotherm of N2 adsorption-desorption of CaO/H-ZSM-5 indicated the type IV isotherm with the presence of hysteresis loop. For the catalytic activity, the biodiesel yield using catalyst of 10 % CaO/HZSM-5 (100 %), 30 % CaO/HZSM-5 (100 %), 50 % CaO/HZSM-5 (100 %) were 24.34, 27.37, and 29.73 %, respectively. It also related with the basic active site, when loading CaO increased, the basic active site also increased. </dc:description>
	<dc:publisher xml:lang="en-US">Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)</dc:publisher>
	<dc:contributor xml:lang="en-US"></dc:contributor>
	<dc:date>2017-12-01</dc:date>
	<dc:type>info:eu-repo/semantics/article</dc:type>
	<dc:type>info:eu-repo/semantics/publishedVersion</dc:type>
	<dc:type xml:lang="en-US"></dc:type>
	<dc:format>application/pdf</dc:format>
	<dc:identifier>https://journal.bcrec.id/index.php/bcrec/article/view/802</dc:identifier>
	<dc:identifier>10.9767/bcrec.12.3.802.329-336</dc:identifier>
	<dc:source xml:lang="en-US">Bulletin of Chemical Reaction Engineering &amp; Catalysis; 2017: BCREC Volume 12 Issue 3 Year 2017 (December 2017); 329-336</dc:source>
	<dc:source>1978-2993</dc:source>
	<dc:language>eng</dc:language>
	<dc:relation>https://journal.bcrec.id/index.php/bcrec/article/view/802/947</dc:relation>
	<dc:relation>https://journal.bcrec.id/index.php/bcrec/article/downloadSuppFile/802/113</dc:relation>
	<dc:rights xml:lang="en-US">Copyright (c) 2017 by Authors, Published by BCREC Group</dc:rights>
	<dc:rights xml:lang="en-US">http://creativecommons.org/licenses/by-sa/4.0</dc:rights>
</oai_dc:dc>