Synthesis of ZnO-Fe3O4 Magnetic Nanocomposites through Sonochemical Methods for Methylene Blue Degradation

Saridewi, Nanda; Komala, Sri; Zulys, Agustino; Nurbayti, Siti; Tulhusna, Latifah; Adawiah, Adawiah

doi:10.9767/bcrec.17.3.15492.650-660

Akses terbuka Jurnal SINTA 1

Synthesis of ZnO-Fe3O4 Magnetic Nanocomposites through Sonochemical Methods for Methylene Blue Degradation

Bulletin of Chemical Reaction Engineering & Catalysis · Vol. ume (2022) · hlm. 650–660

DOI: 10.9767/bcrec.17.3.15492.650-660
ISSN: 1978-2993
Terbit: 2022-09-30
Penerbit: Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)
Bahasa: eng
Lisensi: creativecommons.org/licenses/by-sa/4.0

Abstrak

Textile industry waste can pollute the aquatic environment because it contains dye contaminants with very stable properties that are difficult to degrade naturally. However, dye contaminants degradation can be carried out by photodegradation using ZnO-Fe3O4 magnetic nanocomposite photocatalysts. This study aims to synthesize ZnO-Fe3O4 magnetic nanocomposite through a sonochemical method. Then measure their photocatalytic activity in methylene blue degradation. The best ZnO-Fe3O4 magnetic nanocomposite is made of ZnO:Fe3O4 mass ratio of 4:1 with a crystal size of 31.058 nm, a hexagonal crystal phase and a particle size of 173.23 nm. The ZnO-Fe3O4 magnetic nanocomposites (4:1) provides optimum degradation capacity of methylene blue under halogen lamp irradiation of 99.56 mg/g at pH 13. Furthermore, the ZnO-Fe3O4 magnetic nanocomposites had good stability in 10 cycles reaction with a degradation capacity of 99.24-99.75 mg/g. The photocatalytic degradation of methylene blue by ZnO-Fe3O4 occurs through the formation of free radical species with hydroxyl radicals as the dominant species that play an important role in the degradation process. Copyright © 2022 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0).

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Syarif Hidayatullah State Islamic University Jakarta
University of Indonesia
National Research and Innovation Agency
Universitas Bhayangkara Jakarta Raya
Universitas Mathla'ul Anwar Banten
Pertamina (Indonesia)
Badan Pengkajian dan Penerapan Teknologi
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Rekan penulis	Organisasi	Artikel bersama
Isalmi Aziz	Syarif Hidayatullah State Islamic University Jakarta	22
Dede Sukandar	Syarif Hidayatullah State Islamic University Jakarta	13
Muhammad Shofyan Gunawan	Syarif Hidayatullah State Islamic University Jakarta	8
Farhan Maulana Azhar	Syarif Hidayatullah State Islamic University Jakarta	7
Risma Nur Fitria	Syarif Hidayatullah State Islamic University Jakarta	7
Lisa Adhani	Universitas Bhayangkara Jakarta Raya	5
Wulandari Oktavia	Syarif Hidayatullah State Islamic University Jakarta	5
Nurhasni Nurhasni	Syarif Hidayatullah State Islamic University Jakarta	5
Yulyani Nur Azizah	Syarif Hidayatullah State Islamic University Jakarta	5
Uly Fitria Bale	Syarif Hidayatullah State Islamic University Jakarta	5
Rizka Fadhilla	Syarif Hidayatullah State Islamic University Jakarta	5
Fitri Nur Ramadhan	Syarif Hidayatullah State Islamic University Jakarta	5
Tarso Rudiana	Universitas Mathla'ul Anwar Banten	4
Jarnuzi Gunlazuardi	University of Indonesia	4
Muhammad Derry Luthfi Yudhi	University of Indonesia	4
Rizkha Fadhilla	Syarif Hidayatullah State Islamic University Jakarta	4
Selviana Rustanti	Syarif Hidayatullah State Islamic University Jakarta	4
Farhah Syahidatul Mala	Syarif Hidayatullah State Islamic University Jakarta	4
Adid Adep Dwiatmoko	National Research and Innovation Agency	3
Anna Muawanah	Syarif Hidayatullah State Islamic University Jakarta	3
Badrul Ulum	Syarif Hidayatullah State Islamic University Jakarta	2
Biaunik Niski Kumila	Syarif Hidayatullah State Islamic University Jakarta	2
Wawan Rustyawan	Pertamina (Indonesia)	2
Ridla Bakri	University of Indonesia	2
Saeful Rohman	Badan Pengkajian dan Penerapan Teknologi	2
Shella Fitria	Syarif Hidayatullah State Islamic University Jakarta	2
Salman Farishi	National Research and Innovation Agency	2
Wahyudin Wahyudin	National Research and Innovation Agency	2
Rizka Hadriyani	Syarif Hidayatullah State Islamic University Jakarta	2
Leni Andriyani	Syarif Hidayatullah State Islamic University Jakarta	2
Nur Mahrunnisa	Syarif Hidayatullah State Islamic University Jakarta	2
Lailatul Badriyah	Syarif Hidayatullah State Islamic University Jakarta	1
Puji Lestari	Jenderal Soedirman University	1
Eka Fitriani Ahmad	Bandung Institute of Technology	1

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Sumber metadata: OAI-PMH (metadata jurnal) https://journal.bcrec.id/index.php/bcrec/oai, pertama di-harvest 8 Nov 2026, terakhir terlihat 8 Nov 2026.

Metadata asli (oai_dc)

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	<dc:title xml:lang="en-US">Synthesis of ZnO-Fe3O4 Magnetic Nanocomposites through Sonochemical Methods for Methylene Blue Degradation</dc:title>
	<dc:creator>Saridewi, Nanda</dc:creator>
	<dc:creator>Komala, Sri</dc:creator>
	<dc:creator>Zulys, Agustino</dc:creator>
	<dc:creator>Nurbayti, Siti</dc:creator>
	<dc:creator>Tulhusna, Latifah</dc:creator>
	<dc:creator>Adawiah, Adawiah</dc:creator>
	<dc:subject xml:lang="en-US">ZnO-Fe3O4; magnetic nanocomposite; degradation; photocatalysts; methylene blue</dc:subject>
	<dc:description xml:lang="en-US">Textile industry waste can pollute the aquatic environment because it contains dye contaminants with very stable properties that are difficult to degrade naturally. However, dye contaminants degradation can be carried out by photodegradation using ZnO-Fe3O4 magnetic nanocomposite photocatalysts. This study aims to synthesize ZnO-Fe3O4 magnetic nanocomposite through a sonochemical method. Then measure their photocatalytic activity in methylene blue degradation. The best ZnO-Fe3O4 magnetic nanocomposite is made of ZnO:Fe3O4 mass ratio of 4:1 with a crystal size of 31.058 nm, a hexagonal crystal phase and a particle size of 173.23 nm. The ZnO-Fe3O4 magnetic nanocomposites (4:1) provides optimum degradation capacity of methylene blue under halogen lamp irradiation of 99.56 mg/g at pH 13. Furthermore, the ZnO-Fe3O4 magnetic nanocomposites had good stability in 10 cycles reaction with a degradation capacity of 99.24-99.75 mg/g. The photocatalytic degradation of methylene blue by ZnO-Fe3O4 occurs through the formation of free radical species with hydroxyl radicals as the dominant species that play an important role in the degradation process. Copyright © 2022 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0). </dc:description>
	<dc:publisher xml:lang="en-US">Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)</dc:publisher>
	<dc:date>2022-09-30</dc:date>
	<dc:type>info:eu-repo/semantics/article</dc:type>
	<dc:type>info:eu-repo/semantics/publishedVersion</dc:type>
	<dc:type xml:lang="en-US"></dc:type>
	<dc:format>application/pdf</dc:format>
	<dc:identifier>https://journal.bcrec.id/index.php/bcrec/article/view/15492</dc:identifier>
	<dc:identifier>10.9767/bcrec.17.3.15492.650-660</dc:identifier>
	<dc:source xml:lang="en-US">Bulletin of Chemical Reaction Engineering &amp; Catalysis; 2022: BCREC Volume 17 Issue 3 Year 2022 (September 2022); 650-660</dc:source>
	<dc:source>1978-2993</dc:source>
	<dc:language>eng</dc:language>
	<dc:relation>https://journal.bcrec.id/index.php/bcrec/article/view/15492/7998</dc:relation>
	<dc:rights xml:lang="en-US">Copyright (c) 2022 by Authors, Published by BCREC Group</dc:rights>
	<dc:rights xml:lang="en-US">https://creativecommons.org/licenses/by-sa/4.0</dc:rights>
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