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Effect of Precursor and Temperature Annealing on the Catalytic Activity of Intermetallic Ni3Sn2 Alloy

Bulletin of Chemical Reaction Engineering & Catalysis · Vol. ume (2022) · hlm. 743–754

DOI
10.9767/bcrec.17.4.15923.743-754
ISSN
1978-2993
Terbit
2022-12-30
Penerbit
Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)
Bahasa
eng
Lisensi
creativecommons.org/licenses/by-sa/4.0

Abstrak

The effect of nickel precursors and the temperature annealing to obtain intermetallic Ni3Sn2 alloy catalysts on its activity and selectivity in the selective hydrogenation of biomass-derived furfural (FFald) were investigated. Two types of nickel precursors (c.a., i) nickel metal (Ni°) derived from Raney®nickel and ii) nickel ion (Ni2+) derived from nickel chloride) were employed as the starting materials via hydrothermal at 423 K for 24 h followed by reduction with H2 at the elevated temperature of 573-873 K for 1.5 h. The physico-chemical properties of the intermetallic Ni3Sn2 were characterized by XRD, N2-, and H2-adsorption, ICP-AES, and NH3-TPD. The intermetallic Ni3Sn2 alloy catalysts, both bulk and supported, demonstrated high activity and selectivity towards hydrogenation of FFald. The activity and selectivity of g-Al2O3 and AA-supported Ni3Sn2 alloy catalysts in the hydrogenation of FFald to furfuryl alcohol (FFalc) were maintained even after annealing at up to 873 K, but that of bulk Ni3Sn2 drastically dropped. Ni-Sn alloy catalysts which were obtained from Raney®Ni precursor showed more stable than that of nickel salts during hydrogenation of furfural to furfuryl alcohol. Copyright © 2022 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0).

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  • Universitas Muhammadiyah Parepare
  • Universitas Halu Oleo
  • IPB University
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Maria Dewi AstutiAfiliasi tidak diketahui6
Sutomo SutomoAfiliasi tidak diketahui5
Edi MikriantoAfiliasi tidak diketahui5
Thea Seventina Desiani BodoiAfiliasi tidak diketahui5
Gagus Ketut SunnardiantoAfiliasi tidak diketahui4
Agung NugrohoAfiliasi tidak diketahui3
Arif RidhoniAfiliasi tidak diketahui3
Ikhsan MustariAfiliasi tidak diketahui3
Anggita NurfitrianiAfiliasi tidak diketahui3
Rahmat Eko SanjayaAfiliasi tidak diketahui3
Eka SuarsoAfiliasi tidak diketahui3
Elisa HayatiAfiliasi tidak diketahui3
Shogo ShimazuAfiliasi tidak diketahui2
Annisa AnnisaIPB University2
Kurnia PutriAfiliasi tidak diketahui2
Astuti Maria DewiAfiliasi tidak diketahui2
Iryanti Fatyasari NataAfiliasi tidak diketahui2
Kiky Corneliasari SembiringAfiliasi tidak diketahui2
Heny Puspita DewiAfiliasi tidak diketahui2
Jayanudin JayanudinAfiliasi tidak diketahui2
Utami IrawatiAfiliasi tidak diketahui2
Shauqi Aulia RifwandaAfiliasi tidak diketahui2
Ferensa OemryAfiliasi tidak diketahui2
Indri Badri AdilinaAfiliasi tidak diketahui2
Takayoshi HaraAfiliasi tidak diketahui2
Andinusa RahmandhikaAfiliasi tidak diketahui1
Ali SaifullahAfiliasi tidak diketahui1
Ali MokhtarAfiliasi tidak diketahui1
Anang KadarsahAfiliasi tidak diketahui1
Dafiuddin SalimAfiliasi tidak diketahui1
Marta DinataAfiliasi tidak diketahui1
Abdullah AbdullahUniversitas Muhammadiyah Parepare1
Susi SusiUniversitas Halu Oleo1
Muhammad Iqbal PratamaAfiliasi tidak diketahui1
Ditya KristinaAfiliasi tidak diketahui1
Dwi Rasy MujiyantiAfiliasi tidak diketahui1

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Sumber metadata: OAI-PMH (metadata jurnal) https://journal.bcrec.id/index.php/bcrec/oai, pertama di-harvest 8 Nov 2026, terakhir terlihat 8 Nov 2026.
Metadata asli (oai_dc) 
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	<dc:title xml:lang="en-US">Effect of Precursor and Temperature Annealing on the Catalytic Activity of Intermetallic Ni3Sn2 Alloy</dc:title>
	<dc:creator>Rodiansono, Rodiansono</dc:creator>
	<dc:creator>Azzahra, Atina Sabila</dc:creator>
	<dc:creator>Husain, Sadang</dc:creator>
	<dc:creator>Ansyah, Pathur Razi</dc:creator>
	<dc:subject xml:lang="en-US">intermetallic Ni3Sn2; bulk structure; supported Ni3Sn2; selective hydrogenation; furfural;</dc:subject>
	<dc:description xml:lang="en-US">The effect of nickel precursors and the temperature annealing to obtain intermetallic Ni3Sn2 alloy catalysts on its activity and selectivity in the selective hydrogenation of biomass-derived furfural (FFald) were investigated. Two types of nickel precursors (c.a., i) nickel metal (Ni°) derived from Raney®nickel and ii) nickel ion (Ni2+) derived from nickel chloride) were employed as the starting materials via hydrothermal at 423 K for 24 h followed by reduction with H2 at the elevated temperature of 573-873 K for 1.5 h. The physico-chemical properties of the intermetallic Ni3Sn2 were characterized by XRD, N2-, and H2-adsorption, ICP-AES, and NH3-TPD. The intermetallic Ni3Sn2 alloy catalysts, both bulk and supported, demonstrated high activity and selectivity towards hydrogenation of FFald. The activity and selectivity of g-Al2O3 and AA-supported Ni3Sn2 alloy catalysts in the hydrogenation of FFald to furfuryl alcohol (FFalc) were maintained even after annealing at up to 873 K, but that of bulk Ni3Sn2 drastically dropped. Ni-Sn alloy catalysts which were obtained from Raney®Ni precursor showed more stable than that of nickel salts during hydrogenation of furfural to furfuryl alcohol. Copyright © 2022 by Authors, Published by BCREC Group. This is an open access article under the CC BY-SA License (https://creativecommons.org/licenses/by-sa/4.0). </dc:description>
	<dc:publisher xml:lang="en-US">Masyarakat Katalis Indonesia - Indonesian Catalyst Society (MKICS)</dc:publisher>
	<dc:date>2022-12-30</dc:date>
	<dc:type>info:eu-repo/semantics/article</dc:type>
	<dc:type>info:eu-repo/semantics/publishedVersion</dc:type>
	<dc:type xml:lang="en-US"></dc:type>
	<dc:format>application/pdf</dc:format>
	<dc:identifier>https://journal.bcrec.id/index.php/bcrec/article/view/15923</dc:identifier>
	<dc:identifier>10.9767/bcrec.17.4.15923.743-754</dc:identifier>
	<dc:source xml:lang="en-US">Bulletin of Chemical Reaction Engineering &amp; Catalysis; 2022: BCREC Volume 17 Issue 4 Year 2022 (December 2022); 743-754</dc:source>
	<dc:source>1978-2993</dc:source>
	<dc:language>eng</dc:language>
	<dc:relation>https://journal.bcrec.id/index.php/bcrec/article/view/15923/8181</dc:relation>
	<dc:relation>https://journal.bcrec.id/index.php/bcrec/article/downloadSuppFile/15923/3860</dc:relation>
	<dc:relation>https://journal.bcrec.id/index.php/bcrec/article/downloadSuppFile/15923/3861</dc:relation>
	<dc:relation>https://journal.bcrec.id/index.php/bcrec/article/downloadSuppFile/15923/3862</dc:relation>
	<dc:relation>https://journal.bcrec.id/index.php/bcrec/article/downloadSuppFile/15923/3863</dc:relation>
	<dc:rights xml:lang="en-US">Copyright (c) 2022 by Authors, Published by BCREC Group</dc:rights>
	<dc:rights xml:lang="en-US">https://creativecommons.org/licenses/by-sa/4.0</dc:rights>
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