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Pillarization of double layer hydroxides using H3[-PW12O40]nH2O: effect of pillarization time

Science and Technology Indonesia · Vol. 2 No. 2 (2017) · hlm. 45–49

DOI
10.26554/sti.2017.2.2.45-49
ISSN
2580-4391, 2580-4405
Terbit
2017-04-10
Penerbit
Research Center of Inorganic Materials and Coordination Complexes, FMIPA Universitas Sriwijaya
Bahasa
eng

Abstrak

The pillarization of Mg/Al double layer hydroxides using polyoxometalate H3[α-PW12O40]·nH2O by comparing the pillarization time i.e. 3 hours, 6 hours, 9 hours, 12 hours, 24 hours, 36 hours and 48 hours has been done. The product of a pillarization was characterized using an FT-IR spectrophotometer and XRD analysis. The result characterization of FT-IR spectrophotometer does not show the optimum of pillarization each time condition. Characterization using XRD shows the optimum pillarization process at 36 hours by showing the existence of double layer hydroxides material at diffraction angle 11.69o deg, 18.30o deg and 34.71o deg. Diffraction in the 60o-63o deg indicates the existence of a pillarization double layer hydroxides. Keywords: Layered double hydroxides, pillarization, polyoxometalate H3[α-PW12O40]·nH2O.

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  • Sriwijaya University
  • Universitas Halu Oleo
  • The University of Western Australia
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Rekan penulisOrganisasiArtikel bersama
Aldes LesbaniSriwijaya University4
Neza Rahayu PalapaSriwijaya University3
Poedji Loekitowati HarianiSriwijaya University2
Salni SalniSriwijaya University2
Tarmizi TaherSriwijaya University2
Muhammad FaizalSriwijaya University2
Aldes LesbaniAfiliasi tidak diketahui2
Busnawir BusnawirUniversitas Halu Oleo1
Hafiludin SamparadjaAfiliasi tidak diketahui1
Addy RachmatSriwijaya University1
Nabila ApriantiSriwijaya University1
Anisa Fitri AmatullahSriwijaya University1
Nurlisa HidayatiSriwijaya University1
Mikha Meilinda ChristinaSriwijaya University1
Ferlinahayati FerlinahayatiSriwijaya University1
Rahfi FarahdibaSriwijaya University1
Adipati NapoleonSriwijaya University1
Bambang YudonoSriwijaya University1
SabaruddinSriwijaya University1
MARYATI BUDI UTAMISriwijaya University1
Yadi UtamaSriwijaya University1
Fitri HadiahSriwijaya University1
Tine ApriantiThe University of Western Australia1
Tuti Indah SariSriwijaya University1
Lora VitanesaSriwijaya University1
Radja Nardo PurbaSriwijaya University1
Intan Permata SariSriwijaya University1
Nurul KholidahSriwijaya University1
Ineke Febrina AnggrainiSriwijaya University1
Risfidian MohadiSriwijaya University1

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Sumber metadata: OAI-PMH (metadata jurnal) http://sciencetechindonesia.com/index.php/jsti/oai, pertama di-harvest 10 Nov 2026, terakhir terlihat 10 Nov 2026.
Metadata asli (oai_dc) 
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	<dc:title xml:lang="en-US">Pillarization of double layer hydroxides using H3[-PW12O40]nH2O: effect of pillarization time</dc:title>
	<dc:creator>Imron, Muhammad</dc:creator>
	<dc:creator>Said, Muhammad</dc:creator>
	<dc:description xml:lang="en-US">The pillarization of Mg/Al double layer hydroxides using polyoxometalate H3[α-PW12O40]·nH2O by comparing the pillarization time i.e. 3 hours, 6 hours, 9 hours, 12 hours, 24 hours, 36 hours and 48 hours has been done. The product of a pillarization was characterized using an FT-IR spectrophotometer and XRD analysis. The result characterization of FT-IR spectrophotometer does not show the optimum of pillarization each time condition. Characterization using XRD shows the optimum pillarization process at 36 hours by showing the existence of double layer hydroxides material at diffraction angle 11.69o deg, 18.30o deg and 34.71o deg. Diffraction in the 60o-63o deg indicates the existence of a pillarization double layer hydroxides. &amp;nbsp;
Keywords: Layered double hydroxides, pillarization, polyoxometalate H3[α-PW12O40]·nH2O.</dc:description>
	<dc:publisher xml:lang="en-US">Research Center of Inorganic Materials and Coordination Complexes, FMIPA Universitas Sriwijaya</dc:publisher>
	<dc:date>2017-04-10</dc:date>
	<dc:type>info:eu-repo/semantics/article</dc:type>
	<dc:type>info:eu-repo/semantics/publishedVersion</dc:type>
	<dc:type xml:lang="en-US">Peer-reviewed Article</dc:type>
	<dc:format>application/pdf</dc:format>
	<dc:identifier>http://sciencetechindonesia.com/index.php/jsti/article/view/17</dc:identifier>
	<dc:identifier>10.26554/sti.2017.2.2.45-49</dc:identifier>
	<dc:source xml:lang="en-US">Science and Technology Indonesia; Vol. 2 No. 2 (2017): April; 45-49</dc:source>
	<dc:source>2580-4391</dc:source>
	<dc:source>2580-4405</dc:source>
	<dc:language>eng</dc:language>
	<dc:relation>http://sciencetechindonesia.com/index.php/jsti/article/view/17/28</dc:relation>
	<dc:rights xml:lang="en-US">Copyright (c) 2017 Science &amp; Technology Indonesia</dc:rights>
</oai_dc:dc>