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Preparation, characterization, and thermal stability of B2O3-ZrO2

Science and Technology Indonesia · Vol. 2 No. 2 (2017) · hlm. 56–58

DOI
10.26554/sti.2017.2.2.56-58
ISSN
2580-4391, 2580-4405
Terbit
2017-04-10
Penerbit
Research Center of Inorganic Materials and Coordination Complexes, FMIPA Universitas Sriwijaya
Bahasa
eng

Abstrak

Synthesis of the borate-based compound with ZrOCl2 to form B2O3-ZrO2 has been conducted. The compound was characterized by FT-IR spectrophotometer, X-ray diffraction, acidity and thermal stability test. The results showed that the FT-IR main vibration spectrum of B2O3-ZrO2 compound has appeared at wave number 401.2 cm-1 for Zr-O bonding vibration, 617.2 cm-1 for B-O-B bonding vibration and 910.4 cm-1 for B-O bonding vibration. The XRD diffraction pattern shows B2O3-ZrO2 compound has an amorphous structure. The FT-IR spectrum after saturated with ammonia and potentiometric titration indicates that the compound of B2O3-ZrO2 has acidic properties with a strong level of acidity. Thermal stability test shows that the B2O3-ZrO2 compounds have high stability on temperature with increasing crystallinity after the compound was heated at 700 °C. Keywords: B2O3-ZrO2, impregnation, thermal stability.

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Aldes LesbaniSriwijaya University16
Neza Rahayu PalapaSriwijaya University7
Alfan WijayaSriwijaya University5
Mardiyanto MardiyantoSriwijaya University5
Nur AhmadSriwijaya University4
Yulizah HanifahSriwijaya University4
Tarmizi TaherSriwijaya University4
Idha RoyaniSriwijaya University3
Hilda ZulkifliSriwijaya University3
Nova YuliasariSriwijaya University2
Amri AmriSriwijaya University2
Sahrul WibiyanSriwijaya University2
Yusuf Mathiinul HakimSriwijaya University2
Arini Fousty BadriSriwijaya University2
NormahSriwijaya University2
Patimah Mega Syah Bahar Nur SiregarSriwijaya University2
Novie JuleantiSriwijaya University2
Eliza ElizaSriwijaya University2
Elfita ElfitaSriwijaya University1
Zaqiya Artha ZaharaSriwijaya University1
Rohmatullaili RohmatullailiSriwijaya University1
Rahma Dinta AstutiSriwijaya University1
Aldes Lesbani Aldes LesbaniAfiliasi tidak diketahui1
Marieska VerawatySriwijaya University1
Agnes AgnesSriwijaya University1
Randi O. SaragihSriwijaya University1
Suheryanto SuheryantoSriwijaya University1
Addy RachmatSriwijaya University1
Bakri Rio RahayuSriwijaya University1
Fitri Suryani ArsyadSriwijaya University1
MardiyantoAfiliasi tidak diketahui1
AmriAfiliasi tidak diketahui1
ElfitaAfiliasi tidak diketahui1
Satria Jaya PriatnaSriwijaya University1
Muhammad Afif AlfariziSriwijaya University1
Siti SailahSriwijaya University1
. MardiantoSriwijaya University1
SuheryantoSriwijaya University1

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Sumber metadata: OAI-PMH (metadata jurnal) http://sciencetechindonesia.com/index.php/jsti/oai, pertama di-harvest 10 Nov 2026, terakhir terlihat 10 Nov 2026.
Metadata asli (oai_dc) 
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	<dc:title xml:lang="en-US">Preparation, characterization, and thermal stability of B2O3-ZrO2</dc:title>
	<dc:creator>Simbolon, Theresia Debora</dc:creator>
	<dc:creator>Mohadi, Risfidian</dc:creator>
	<dc:description xml:lang="en-US">Synthesis of the borate-based compound with ZrOCl2 to form B2O3-ZrO2 has been conducted. The compound was characterized by FT-IR spectrophotometer, X-ray diffraction, acidity and thermal stability test. The results showed that the FT-IR main vibration spectrum of B2O3-ZrO2 compound has appeared at wave number 401.2 cm-1 for Zr-O bonding vibration, 617.2 cm-1 for B-O-B bonding vibration and 910.4 cm-1 for B-O bonding vibration. The XRD diffraction pattern shows B2O3-ZrO2 compound has an amorphous structure. The FT-IR spectrum after saturated with ammonia and potentiometric titration indicates that the compound of B2O3-ZrO2 has acidic properties with a strong level of acidity. Thermal stability test shows that the B2O3-ZrO2 compounds have high stability on temperature with increasing crystallinity after the compound was heated at 700 °C.
Keywords: B2O3-ZrO2, impregnation, thermal stability. &amp;nbsp;</dc:description>
	<dc:publisher xml:lang="en-US">Research Center of Inorganic Materials and Coordination Complexes, FMIPA Universitas Sriwijaya</dc:publisher>
	<dc:date>2017-04-10</dc:date>
	<dc:type>info:eu-repo/semantics/article</dc:type>
	<dc:type>info:eu-repo/semantics/publishedVersion</dc:type>
	<dc:type xml:lang="en-US">Peer-reviewed Article</dc:type>
	<dc:format>application/pdf</dc:format>
	<dc:identifier>http://sciencetechindonesia.com/index.php/jsti/article/view/20</dc:identifier>
	<dc:identifier>10.26554/sti.2017.2.2.56-58</dc:identifier>
	<dc:source xml:lang="en-US">Science and Technology Indonesia; Vol. 2 No. 2 (2017): April; 56-58</dc:source>
	<dc:source>2580-4391</dc:source>
	<dc:source>2580-4405</dc:source>
	<dc:language>eng</dc:language>
	<dc:relation>http://sciencetechindonesia.com/index.php/jsti/article/view/20/29</dc:relation>
	<dc:rights xml:lang="en-US">Copyright (c) 2017 Science &amp; Technology Indonesia</dc:rights>
</oai_dc:dc>