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Characterization Study of Dyes Photodegradation-Adsorption Products by TiO2-Chitosan Immobilized on Glass Beads using Flow System

VALENSI · Vol. ume No. 1 (2023) · hlm. 123–135

DOI
10.15408/jkv.v9i1.31855
ISSN
2548-3013, 2460-6065
Terbit
2023-06-04
Penerbit
Department of Chemistry, Faculty of Science and Technology Syarif Hidayatullah Jakarta State Islamic University
Bahasa
eng

Abstrak

Dyes have a complex molecular structure that is difficult to degrade and can persist for a long time in water bodies. This study examines more thoroughly the effectiveness of photodegradation-adsorption of dyes, kinetic aspects, isotherms, thermodynamics, identification of the structure of photodegradation products, and changes in environmental quality parameter values whose results are quite satisfactory. The combination of photodegradation-adsorption of dyes by TiO2-chitosan modified glass beads using a flow system has never been accomplished before. Flowing of the dye resulted in a dye degradation efficiency of 99%. The FESEM-EDX analysis shows that TiO2-chitosan has been coated onto the surface of the glass beads. R2 of kinetics MB, MO, RB are 0.99234, 0.9889, 0.9971, which were pseudo-first order. Qm, KL, R2 are 6.4382, 0.70533, 0.99923; 16.7364, 1.42059, 0.98816; 6.0078, 1.06973, 0.99889, respectively. The ∆H, ∆S, ∆S of -9.388, -0.024, -1.979; -27.182, -0.078, -3.592; -4.819, -0.017, 0.464 indicate the exothermic and spontaneous reaction. COD, TOC, pH, turbidity values have reached the threshold required by the government. The degradation products formed during the photodegradation-adsorption process were identified using LC-MS that the structure of the dye has been degraded to become simpler so that it is safely disposed of into the environment.

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  • Andalas University
  • Universitas Jenderal Achmad Yani
  • Bandung Institute of Technology
  • National Nuclear Energy Agency of Indonesia
  • University of Indonesia
  • National Research and Innovation Agency
  • Institut Teknologi Sepuluh Nopember
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Rekan penulisOrganisasiArtikel bersama
Safni SafniAndalas University3
Yulia Eka PutriAndalas University2
Upita SeptianiAndalas University2
Reza Audina PutriAndalas University2
S. AnwarIndonesia University of Education1
Meri SuhartiniNational Nuclear Energy Agency of Indonesia1
S SudirmanNational Nuclear Energy Agency of Indonesia1
Santoso PrayitnoNational Nuclear Energy Agency of Indonesia1
Budi Indra SetiawanIPB University1
U. ZhafirahUniversity of Indonesia1
Indah PermatasariSriwijaya University1
Nofebriani DinaAndalas University1
Nurul PratiwiAndalas University1
Atthar Luqman IvansyahBandung Institute of Technology1
Yuly KusumawatiInstitut Teknologi Sepuluh Nopember1
Evan AttalarioAndalas University1
Resha Mutia RahmaInstitut Teknologi Sepuluh Nopember1
Anceu MurniatiUniversitas Jenderal Achmad Yani1
Jasmansyah JasmansyahUniversitas Jenderal Achmad Yani1
Arie HardianUniversitas Jenderal Achmad Yani1
Atiek Rostika NoviyantiPadjadjaran University1
Muhammad RezaBandung Institute of Technology1
Yanuar SetiadiNational Nuclear Energy Agency of Indonesia1
Farah Nur FauziyahUniversitas Jenderal Achmad Yani1
Teguh KaryaUniversitas Jenderal Achmad Yani1
Dani Gustaman SyarifNational Research and Innovation Agency1
Ismunandar IsmunandarBandung Institute of Technology1
Kiki Adi KurniaAfiliasi tidak diketahui1
Wahju TjahjaningsihAfiliasi tidak diketahui1
PatmawatiAfiliasi tidak diketahui1
Ina Salwany Md YasinAfiliasi tidak diketahui1
Woro Hastuti SatyantiniAfiliasi tidak diketahui1
Ainun Kurnia IzzataAfiliasi tidak diketahui1
Woro Hastuti SatyantiniUniversitas Airlangga1
Ainun Kurnia IzzataUniversitas Airlangga1

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Sumber metadata: OAI-PMH (metadata jurnal) http://journal.uinjkt.ac.id/index.php/valensi/oai, pertama di-harvest 10 Nov 2026, terakhir terlihat 10 Nov 2026.
Metadata asli (oai_dc) 
<oai_dc:dc xmlns="http://www.openarchives.org/OAI/2.0/" xmlns:dc="http://purl.org/dc/elements/1.1/" xmlns:oai_dc="http://www.openarchives.org/OAI/2.0/oai_dc/" xmlns:xsi="http://www.w3.org/2001/XMLSchema-instance" xsi:schemaLocation="http://www.openarchives.org/OAI/2.0/oai_dc/  http://www.openarchives.org/OAI/2.0/oai_dc.xsd">
	<dc:title xml:lang="en">Characterization Study of Dyes Photodegradation-Adsorption Products by TiO2-Chitosan Immobilized on Glass Beads using Flow System</dc:title>
	<dc:creator xml:lang="en">Mahadika, Bella Sukma</dc:creator>
	<dc:creator xml:lang="en">Saefumillah, Asep</dc:creator>
	<dc:creator xml:lang="en">Saepurahman, Saepurahman</dc:creator>
	<dc:creator xml:lang="en">Kurnia, Kiki Adi</dc:creator>
	<dc:creator xml:lang="en">Wellia, Diana Vanda</dc:creator>
	<dc:subject xml:lang="en">Degradation product</dc:subject>
	<dc:subject xml:lang="en">dyes</dc:subject>
	<dc:subject xml:lang="en">TiO2</dc:subject>
	<dc:subject xml:lang="en">chitosan</dc:subject>
	<dc:subject xml:lang="en">glass beads</dc:subject>
	<dc:description xml:lang="en">Dyes have a complex molecular structure that is difficult to degrade and can persist for a long time in water bodies. This study examines more thoroughly the effectiveness of photodegradation-adsorption of dyes, kinetic aspects, isotherms, thermodynamics, identification of the structure of photodegradation products, and changes in environmental quality parameter values whose results are quite satisfactory. The combination of photodegradation-adsorption of dyes by TiO2-chitosan modified glass beads using a flow system has never been accomplished before. Flowing of the dye resulted in a dye degradation efficiency of 99%. The FESEM-EDX analysis shows that TiO2-chitosan has been coated onto the surface of the glass beads. R2 of kinetics MB, MO, RB are 0.99234, 0.9889, 0.9971, which were pseudo-first order. Qm, KL, R2 are 6.4382, 0.70533, 0.99923; 16.7364, 1.42059, 0.98816; 6.0078, 1.06973, 0.99889, respectively. The ∆H, ∆S, ∆S of -9.388, -0.024, -1.979; -27.182, -0.078, -3.592; -4.819, -0.017, 0.464 indicate the exothermic and spontaneous reaction. COD, TOC, pH, turbidity values have reached the threshold required by the government. The degradation products formed during the photodegradation-adsorption process were identified using LC-MS that the structure of the dye has been degraded to become simpler so that it is safely disposed of into the environment.</dc:description>
	<dc:publisher xml:lang="en">Department of Chemistry, Faculty of Science and Technology Syarif Hidayatullah Jakarta State Islamic University</dc:publisher>
	<dc:date>2023-06-04</dc:date>
	<dc:type>info:eu-repo/semantics/article</dc:type>
	<dc:type>info:eu-repo/semantics/publishedVersion</dc:type>
	<dc:format>application/pdf</dc:format>
	<dc:format>application/pdf</dc:format>
	<dc:identifier>https://journal.uinjkt.ac.id/index.php/valensi/article/view/31855</dc:identifier>
	<dc:identifier>10.15408/jkv.v9i1.31855</dc:identifier>
	<dc:source xml:lang="en">Jurnal Kimia Valensi; Jurnal Kimia VALENSI Volume 9, No. 1, May 2023; 123-135</dc:source>
	<dc:source>2548-3013</dc:source>
	<dc:source>2460-6065</dc:source>
	<dc:language>eng</dc:language>
	<dc:relation>https://journal.uinjkt.ac.id/index.php/valensi/article/view/31855/pdf</dc:relation>
	<dc:relation>https://journal.uinjkt.ac.id/index.php/valensi/article/view/31855/17141</dc:relation>
	<dc:rights xml:lang="en">Copyright (c) 2023 Bella Sukma Mahadika</dc:rights>
</oai_dc:dc>