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Fabrication of Calcite Calcium Carbonate from Eggshells Biogenic Waste Through Carbonation Method

VALENSI · Vol. ume No. 1 (2025) · hlm. 9–17

DOI
10.15408/jkv.v11i1.41914
ISSN
2548-3013, 2460-6065
Terbit
2025-05-31
Penerbit
Department of Chemistry, Faculty of Science and Technology Syarif Hidayatullah Jakarta State Islamic University
Bahasa
eng
Lisensi
creativecommons.org/licenses/by-sa/4.0

Abstrak

Calcium carbonate derived from eggshells has significant potential for use in drug delivery systems, pharmaceutical, food, catalyst, cement, and concrete industries. Although eggshell waste is non-toxic, its excessive accumulation in the environment may contribute to ecological issues. Colonizing pathogenic bacteria in unprocessed eggshell waste poses a potential health risk. The present study outlines the production of precipitated calcium carbonate (PCC) from eggshell waste through a calcination-carbonation process, offering a sustainable approach to its utilization. The calcination was carried out at 900 ºC. The carbonation process was performed in an HNO3 solution, and the NH3 solution was under-treated for 60 minutes. The results exhibited that the precipitated calcium carbonate (PCC) had a purity of 95.2% CaO. It possessed predominantly the calcite phase with a rhombohedral crystal system, as confirmed by the XRD analysis. The crystallite size of PCC was 109.5 nm, measured using the Debye-Scherrer equation. The phase composition of PCC was 99.3% calcite, 0.5% vaterite, and 0.2% aragonite. FTIR analysis further corroborated this data by showing a sharp and unsplit peak at 1419 cm-1, demonstrating the presence of a calcite phase. SEM images revealed a cubic-like morphology, a characteristic of the calcite form of calcium carbonate (CaCO3). The synthesized calcium carbonate in this study holds potential for applications in dental materials and as fillers in polymer matrices for food packaging.

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  • Universitas Gadjah Mada
  • Sumatera Institute of Technology
  • Muhammadiyah University of Yogyakarta
  • National Research and Innovation Agency
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Rekan penulisOrganisasiArtikel bersama
Dyah IrnawatiUniversitas Gadjah Mada4
Ema MulyawatiUniversitas Gadjah Mada3
Juni HandajaniUniversitas Gadjah Mada2
Widowati SiswomihardjoUniversitas Gadjah Mada2
Widya AsmaraUniversitas Gadjah Mada2
Tunjung NugraheniUniversitas Gadjah Mada2
B. F. Y. SerliSumatera Institute of Technology1
Nur AdlianiSumatera Institute of Technology1
Chairunnisa ChairunnisaSumatera Institute of Technology1
Yuni LisafitriSumatera Institute of Technology1
Niswati Fathmah RosyidaUniversitas Gadjah Mada1
Pinandi Sri PudyaniUniversitas Gadjah Mada1
Marsetyawan H. N. E. SoesatyoUniversitas Gadjah Mada1
Archadian NuryantiUniversitas Gadjah Mada1
Dewi AgustinaUniversitas Gadjah Mada1
Yulita KristantiUniversitas Gadjah Mada1
Marsetyawan HnesUniversitas Gadjah Mada1
Alizatul Khairani HasanUniversitas Gadjah Mada1
Sri Kavi SubramaniamUniversitas Gadjah Mada1
Widjijono WidjijonoUniversitas Gadjah Mada1
Dwi Aji NugrohoMuhammadiyah University of Yogyakarta1
Wijayanti Dwi AastutiUniversitas Gadjah Mada1
Dana ArdianataMuhammadiyah University of Yogyakarta1
Dyah Anindya WidyasriniUniversitas Gadjah Mada1
Wayan Tunas ArtamaUniversitas Gadjah Mada1
Sri Budi BarunawatiUniversitas Gadjah Mada1
Suparyono SalehUniversitas Gadjah Mada1
Yosi Bayu MurtiUniversitas Gadjah Mada1
HarsiniUniversitas Gadjah Mada1
WidjijonoUniversitas Gadjah Mada1
Mohammad Imanuddin YasnawiUniversitas Gadjah Mada1
Dhea Maurilla VeraniUniversitas Gadjah Mada1
Yuichi KamiyaAfiliasi tidak diketahui1
Adhi Dwi HatmantoUniversitas Gadjah Mada1
Rakhma Amalia NurdinaUniversitas Gadjah Mada1

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Sumber metadata: OAI-PMH (metadata jurnal) http://journal.uinjkt.ac.id/index.php/valensi/oai, pertama di-harvest 10 Nov 2026, terakhir terlihat 10 Nov 2026.
Metadata asli (oai_dc) 
<oai_dc:dc xmlns="http://www.openarchives.org/OAI/2.0/" xmlns:dc="http://purl.org/dc/elements/1.1/" xmlns:oai_dc="http://www.openarchives.org/OAI/2.0/oai_dc/" xmlns:xsi="http://www.w3.org/2001/XMLSchema-instance" xsi:schemaLocation="http://www.openarchives.org/OAI/2.0/oai_dc/  http://www.openarchives.org/OAI/2.0/oai_dc.xsd">
	<dc:title xml:lang="en">Fabrication of Calcite Calcium Carbonate from Eggshells Biogenic Waste Through Carbonation Method</dc:title>
	<dc:creator xml:lang="en">Mariyam, Mariyam</dc:creator>
	<dc:creator xml:lang="en">Sunarintyas, Siti </dc:creator>
	<dc:creator xml:lang="en">Yuliatun, Leny </dc:creator>
	<dc:creator xml:lang="en">Khuzaimah, Ismi </dc:creator>
	<dc:creator xml:lang="en">Nuryono, Nuryono</dc:creator>
	<dc:subject xml:lang="en">CaCO3</dc:subject>
	<dc:subject xml:lang="en">calcite</dc:subject>
	<dc:subject xml:lang="en">carbonation</dc:subject>
	<dc:subject xml:lang="en">eggshell</dc:subject>
	<dc:subject xml:lang="en">synthesis</dc:subject>
	<dc:description xml:lang="en">Calcium carbonate derived from eggshells has significant potential for use in drug delivery systems, pharmaceutical, food, catalyst, cement, and concrete industries. Although eggshell waste is non-toxic, its excessive accumulation in the environment may contribute to ecological issues. Colonizing pathogenic bacteria in unprocessed eggshell waste poses a potential health risk. The present study outlines the production of precipitated calcium carbonate (PCC) from eggshell waste through a calcination-carbonation process, offering a sustainable approach to its utilization. The calcination was carried out at 900 ºC. The carbonation process was performed in an HNO3 solution, and the NH3 solution was under-treated for 60 minutes. The results exhibited that the precipitated calcium carbonate (PCC) had a purity of 95.2% CaO. It possessed predominantly the calcite phase with a rhombohedral crystal system, as confirmed by the XRD analysis. The crystallite size of PCC was 109.5 nm, measured using the Debye-Scherrer equation. The phase composition of PCC was 99.3% calcite, 0.5% vaterite, and 0.2% aragonite. FTIR analysis further corroborated this data by showing a sharp and unsplit peak at 1419 cm-1, demonstrating the presence of a calcite phase. SEM images revealed a cubic-like morphology, a characteristic of the calcite form of calcium carbonate (CaCO3). The synthesized calcium carbonate in this study holds potential for applications in dental materials and as fillers in polymer matrices for food packaging.</dc:description>
	<dc:publisher xml:lang="en">Department of Chemistry, Faculty of Science and Technology Syarif Hidayatullah Jakarta State Islamic University</dc:publisher>
	<dc:date>2025-05-31</dc:date>
	<dc:type>info:eu-repo/semantics/article</dc:type>
	<dc:type>info:eu-repo/semantics/publishedVersion</dc:type>
	<dc:format>application/pdf</dc:format>
	<dc:identifier>https://journal.uinjkt.ac.id/index.php/valensi/article/view/41914</dc:identifier>
	<dc:identifier>10.15408/jkv.v11i1.41914</dc:identifier>
	<dc:source xml:lang="en">Jurnal Kimia Valensi; Jurnal Kimia VALENSI,  Volume 11, No. 1, May 2025; 9-17</dc:source>
	<dc:source>2548-3013</dc:source>
	<dc:source>2460-6065</dc:source>
	<dc:language>eng</dc:language>
	<dc:relation>https://journal.uinjkt.ac.id/index.php/valensi/article/view/41914/17958</dc:relation>
	<dc:rights xml:lang="en">Copyright (c) 2025 Mariyam Mariyam</dc:rights>
	<dc:rights xml:lang="en">https://creativecommons.org/licenses/by-sa/4.0</dc:rights>
</oai_dc:dc>