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Synthesis and Characterization of Copoly(Anethole-Stearyl Acrylate) as Phenol Adsorbent

VALENSI · Vol. ume No. 2 (2025) · hlm. 217–225

DOI
10.15408/jkv.v11i2.46484
ISSN
2548-3013, 2460-6065
Terbit
2025-11-30
Penerbit
Department of Chemistry, Faculty of Science and Technology Syarif Hidayatullah Jakarta State Islamic University
Bahasa
eng
Lisensi
creativecommons.org/licenses/by-sa/4.0

Abstrak

This study aims to synthesize copoly (Anethole-stearyl acrylate, SA) through cationic polymerization at room temperature (28–36°C) under a nitrogen atmosphere. The synthesis was carried out without a solvent using BF3O(C2H5)2 as the initiator. SA was added in varying weights of 2%, 4%, and 6% relative to anethole. The product obtained from the synthesis was then applied as a phenol adsorbent using the batch method at different contact times. FTIR (Fourier Transform Infrared) analysis showed that methoxy group (-OCH3) termination occurred at wavenumber 1147 cm-1, followed by the loss of vinyl group (C=C) at 1633–1654 cm-1. In addition, the loss of =C-H vinyl bending and stretching group absorption occurred at 964–998 cm-1 and 3025–3095 cm-1, respectively. Structural analysis using 1H-NMR showed the loss of the vinyl group proton signal at a chemical shift (δH) of 5.8–39 ppm. The addition of 2%, 4%, and 6% SA led to an increase in intrinsic viscosity of 26.891, 41.093, and 55.336, respectively. The morphology of copoly showed the presence of various cavities. The degradation temperature of the product increased with the addition of SA. During the application of copoly as a phenol adsorbent, the 6% (w/w) concentration had the largest adsorption capacity of 2.22 mg/g.

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  • Sebelas Maret University
  • Institut Teknologi Sepuluh Nopember
  • Institut Ilmu Kesehatan Bhakti Wiyata
  • University of Miyazaki
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Rekan penulisOrganisasiArtikel bersama
Venty SuryantiSebelas Maret University3
Atmira SariwatiInstitut Ilmu Kesehatan Bhakti Wiyata2
Fita SariInstitut Ilmu Kesehatan Bhakti Wiyata2
Betty NurhayatiSebelas Maret University1
Candra PurnawanSebelas Maret University1
Ozi Adi SaputraSebelas Maret University1
KurniaSebelas Maret University1
Septi PujiasihSebelas Maret University1
Vanani Nur RizkiSebelas Maret University1
Hamzah FansuriInstitut Teknologi Sepuluh Nopember1
Witri Wahyu LestariSebelas Maret University1
Triyanda GunawanInstitut Teknologi Sepuluh Nopember1
Jeesica Hermayanti PratamaInstitut Teknologi Sepuluh Nopember1
Burhan Fatkhur RahmanSebelas Maret University1
Fauziyah AzhariSebelas Maret University1
Nurul WidiastutiInstitut Teknologi Sepuluh Nopember1
Shinta Amelia PutriSebelas Maret University1
Hamdan Dwi RisqiAfiliasi tidak diketahui1
Ichiro KameiUniversity of Miyazaki1
Ninis YuliatiInstitut Ilmu Kesehatan Bhakti Wiyata1
Fajar Rakhman WibowoSebelas Maret University1
Maulidan FirdausSebelas Maret University1
Triana KusumaningsihSebelas Maret University1
Alfia Uke TaharaSebelas Maret University1
Soerya Dewi MarliyanaSebelas Maret University1
Muhammad Widyo WartonoSebelas Maret University1
Fitria RahmawatiSebelas Maret University1
Chintya DewiSebelas Maret University1

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Sumber metadata: OAI-PMH (metadata jurnal) http://journal.uinjkt.ac.id/index.php/valensi/oai, pertama di-harvest 10 Nov 2026, terakhir terlihat 10 Nov 2026.
Metadata asli (oai_dc) 
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	<dc:title xml:lang="en">Synthesis and Characterization of Copoly(Anethole-Stearyl Acrylate) as Phenol Adsorbent</dc:title>
	<dc:creator xml:lang="en">Handayani, Desi Suci</dc:creator>
	<dc:creator xml:lang="en">Pramono, Edi </dc:creator>
	<dc:creator xml:lang="en">Dewi, Anita Kusuma</dc:creator>
	<dc:subject xml:lang="en">Adsorbent</dc:subject>
	<dc:subject xml:lang="en">anethole</dc:subject>
	<dc:subject xml:lang="en">cationic copolymerization</dc:subject>
	<dc:subject xml:lang="en">total phenol</dc:subject>
	<dc:subject xml:lang="en">stearyl acrylate</dc:subject>
	<dc:description xml:lang="en">This study aims to synthesize copoly (Anethole-stearyl acrylate, SA) through cationic polymerization at room temperature (28–36°C) under a nitrogen atmosphere. The synthesis was carried out without a solvent using BF3O(C2H5)2 as the initiator. SA was added in varying weights of 2%, 4%, and 6% relative to anethole. The product obtained from the synthesis was then applied as a phenol adsorbent using the batch method at different contact times. FTIR (Fourier Transform Infrared) analysis showed that methoxy group (-OCH3) termination occurred at wavenumber 1147 cm-1, followed by the loss of vinyl group (C=C) at 1633–1654 cm-1. In addition, the loss of =C-H vinyl bending and stretching group absorption occurred at 964–998 cm-1 and 3025–3095 cm-1, respectively. Structural analysis using 1H-NMR showed the loss of the vinyl group proton signal at a chemical shift (δH) of 5.8–39 ppm. The addition of 2%, 4%, and 6% SA led to an increase in intrinsic viscosity of 26.891, 41.093, and 55.336, respectively. The morphology of copoly showed the presence of various cavities. The degradation temperature of the product increased with the addition of SA. During the application of copoly as a phenol adsorbent, the 6% (w/w) concentration had the largest adsorption capacity of 2.22 mg/g.</dc:description>
	<dc:publisher xml:lang="en">Department of Chemistry, Faculty of Science and Technology Syarif Hidayatullah Jakarta State Islamic University</dc:publisher>
	<dc:date>2025-11-30</dc:date>
	<dc:type>info:eu-repo/semantics/article</dc:type>
	<dc:type>info:eu-repo/semantics/publishedVersion</dc:type>
	<dc:format>application/pdf</dc:format>
	<dc:identifier>https://journal.uinjkt.ac.id/index.php/valensi/article/view/46484</dc:identifier>
	<dc:identifier>10.15408/jkv.v11i2.46484</dc:identifier>
	<dc:source xml:lang="en">Jurnal Kimia Valensi; Jurnal Kimia VALENSI,  Volume 11, No. 2, November 2025; 217-225</dc:source>
	<dc:source>2548-3013</dc:source>
	<dc:source>2460-6065</dc:source>
	<dc:language>eng</dc:language>
	<dc:relation>https://journal.uinjkt.ac.id/index.php/valensi/article/view/46484/18403</dc:relation>
	<dc:rights xml:lang="en">Copyright (c) 2025 Desi Suci Handayani, Edi Pramono, Anita Kusuma Dewi</dc:rights>
	<dc:rights xml:lang="en">https://creativecommons.org/licenses/by-sa/4.0</dc:rights>
</oai_dc:dc>