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Synthesis and Characterization of the Microstructure and Functional Group Bond of Fe3o4 Nanoparticles from Natural Iron Sand in Tobelo North Halmahera

JURNAL ILMIAH PENDIDIKAN FISIKA AL BIRUNI · Vol. 7 No. 2 (2018) · pp. 129–138

DOI
10.24042/jipfalbiruni.v7i2.2913
ISSN
2503-023X, 2303-1832
Published
2018-10-28
Publisher
Universitas Islam Negeri Raden Intan Lampung, Indonesia
Language
eng

Abstract

The Fe3O4 nanoparticles have been successfully synthesized from natural iron sand by using co-precipitation method at a temperature of 56oC. The elemental identification, structural characterization, and bonding analysis were carried out using XRF, XRD, and FTIR, respectively. The sample nanoparticles contain elements of Al, P, Ca, Ti, V, Cr, Mn, Ni, Cu, Zn, Rb, Re, Bi, and Fe. The composition of Fe element is 87.37%. The sample of the nanoparticle exhibited as the Fe3O4 which was shown by the diffraction pattern that belongs to a cubic spinel structure of Fe3O4. The crystallite size of the nanoparticle is 42.25 ± 0.42 nm. The lattice parameter was found at 8.384 ± 0.049 Å. The crystallite density is 5.232 103 kg/m3 while the lattice strain is 1.413 10-3/line. The FTIR spectra confirm that the existence of Fe-O stretching vibration in the range frequency of 658 cm-1-506 cm-1

Keywords

Collaboration network of the authors

26 authors · 72 co-authorship links

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  • Hasanuddin University
  • Universitas Halu Oleo
  • Institut Agama Islam Negeri Kendari
  • Kwansei Gakuin University
  • Affiliation unknown
  • Different organisations
  • Same organisation
  • Affiliation unknown
  • Thicker line = more joint articles · bigger circle = more articles
Show as table
Co-authorOrganisationJoint articles
Bayu Achil SadjabAffiliation unknown2
Takeshi KatoAffiliation unknown2
Satoshi IwataAffiliation unknown2
Hafied CangaraHasanuddin University1
Yumnawati YumnawatiAffiliation unknown1
Ismail SalehUniversitas Halu Oleo1
Abdin AbdinAffiliation unknown1
La AgusuAffiliation unknown1
La Ode RusmanAffiliation unknown1
Adrian Rahmat NurAffiliation unknown1
Kurnia KurniaInstitut Agama Islam Negeri Kendari1
Novita KundimanAffiliation unknown1
Joko UtomoAffiliation unknown1
Lintang GriyanikaAffiliation unknown1
Ayu Kurnia AgustinaAffiliation unknown1
Diah MahmudahAffiliation unknown1
Nurhidayati SakinahAffiliation unknown1
Eko Arief SetiadiAffiliation unknown1
Nanda ShabrinaAffiliation unknown1
Hesti Retno Budi UtamiAffiliation unknown1
Nur Fadhilah FahmiAffiliation unknown1
Rofiqul UmamKwansei Gakuin University1
Steven IwamonyAffiliation unknown1

Affiliations come from OpenAlex; journal OAI-PMH metadata carries none. Authors without an OpenAlex ID are matched by name, which can merge or split people.

Metadata source: OAI-PMH (metadata jurnal) http://ejournal.radenintan.ac.id/index.php/al-biruni/oai, first harvested 9 Nov 2026, last seen 9 Nov 2026.
Original metadata (oai_dc) 
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	<dc:title xml:lang="en">Synthesis and Characterization of the Microstructure and Functional Group Bond of Fe3o4 Nanoparticles from Natural Iron Sand in Tobelo North Halmahera</dc:title>
	<dc:creator xml:lang="en">Malega, Ferni</dc:creator>
	<dc:creator xml:lang="en">Indrayana, I Putu Tedy</dc:creator>
	<dc:creator xml:lang="en">Suharyadi, Edi</dc:creator>
	<dc:subject xml:lang="en">characterization</dc:subject>
	<dc:subject xml:lang="en">coprecipitation</dc:subject>
	<dc:subject xml:lang="en">microstructure</dc:subject>
	<dc:subject xml:lang="en">iron sand</dc:subject>
	<dc:subject xml:lang="en">synthesis</dc:subject>
	<dc:description xml:lang="en">The Fe3O4 nanoparticles have been successfully synthesized from natural iron sand by using co-precipitation method at a temperature of 56oC. The elemental identification, structural characterization, and bonding analysis were carried out using XRF, XRD, and FTIR, respectively. The sample nanoparticles contain elements of Al, P, Ca, Ti, V, Cr, Mn, Ni, Cu, Zn, Rb, Re, Bi, and Fe. The composition of Fe element is 87.37%. The sample of the nanoparticle exhibited as the Fe3O4 which was shown by the diffraction pattern that belongs to a cubic spinel structure of Fe3O4. The crystallite size of the nanoparticle is 42.25 ± 0.42 nm. The lattice parameter was found at 8.384 ± 0.049 Å. The crystallite density is 5.232 103 kg/m3 while the lattice strain is 1.413 10-3/line. The FTIR spectra confirm that the existence of Fe-O stretching vibration in the range frequency of 658 cm-1-506 cm-1</dc:description>
	<dc:publisher xml:lang="en">Universitas Islam Negeri Raden Intan Lampung, Indonesia</dc:publisher>
	<dc:date>2018-10-28</dc:date>
	<dc:type>info:eu-repo/semantics/article</dc:type>
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	<dc:type xml:lang="en">Peer-reviewed Article</dc:type>
	<dc:format>application/pdf</dc:format>
	<dc:format>application/msword</dc:format>
	<dc:identifier>https://ejournal.radenintan.ac.id/index.php/al-biruni/article/view/2913</dc:identifier>
	<dc:identifier>10.24042/jipfalbiruni.v7i2.2913</dc:identifier>
	<dc:source xml:lang="en">Jurnal Ilmiah Pendidikan Fisika Al-Biruni; Vol. 7 No. 2 (2018): Jurnal Ilmiah pendidikan Fisika Al-Biruni; 129-138</dc:source>
	<dc:source xml:lang="id">Jurnal Ilmiah Pendidikan Fisika Al-Biruni; Vol 7 No 2 (2018): Jurnal Ilmiah pendidikan Fisika Al-Biruni; 129-138</dc:source>
	<dc:source>2503-023X</dc:source>
	<dc:source>2303-1832</dc:source>
	<dc:language>eng</dc:language>
	<dc:relation>https://ejournal.radenintan.ac.id/index.php/al-biruni/article/view/2913/pdf</dc:relation>
	<dc:relation>https://ejournal.radenintan.ac.id/index.php/al-biruni/article/view/2913/8282</dc:relation>
	<dc:rights xml:lang="en">Copyright (c) 2018 Jurnal Ilmiah Pendidikan Fisika Al-Biruni</dc:rights>
</oai_dc:dc>