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Preparation, characterization, and thermal stability of B2O3-ZrO2

Science and Technology Indonesia · Vol. 2 No. 2 (2017) · pp. 56–58

DOI
10.26554/sti.2017.2.2.56-58
ISSN
2580-4391, 2580-4405
Published
2017-04-10
Publisher
Research Center of Inorganic Materials and Coordination Complexes, FMIPA Universitas Sriwijaya
Language
eng

Abstract

Synthesis of the borate-based compound with ZrOCl2 to form B2O3-ZrO2 has been conducted. The compound was characterized by FT-IR spectrophotometer, X-ray diffraction, acidity and thermal stability test. The results showed that the FT-IR main vibration spectrum of B2O3-ZrO2 compound has appeared at wave number 401.2 cm-1 for Zr-O bonding vibration, 617.2 cm-1 for B-O-B bonding vibration and 910.4 cm-1 for B-O bonding vibration. The XRD diffraction pattern shows B2O3-ZrO2 compound has an amorphous structure. The FT-IR spectrum after saturated with ammonia and potentiometric titration indicates that the compound of B2O3-ZrO2 has acidic properties with a strong level of acidity. Thermal stability test shows that the B2O3-ZrO2 compounds have high stability on temperature with increasing crystallinity after the compound was heated at 700 °C. Keywords: B2O3-ZrO2, impregnation, thermal stability.

Collaboration network of the authors

40 authors · 176 co-authorship links · showing the 40 most connected

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Co-authorOrganisationJoint articles
Aldes LesbaniAffiliation unknown19
Neza Rahayu PalapaAffiliation unknown8
Alfan WijayaAffiliation unknown5
nur AhmadAffiliation unknown5
Mardiyanto MardiyantoAffiliation unknown5
Tarmizi TaherAffiliation unknown5
Yulizah HanifahAffiliation unknown4
Eliza ElizaAffiliation unknown3
Idha RoyaniAffiliation unknown3
Amri AmriAffiliation unknown3
Hilda ZulkifliAffiliation unknown3
Nurlisa HidayatiAffiliation unknown2
Nova YuliasariAffiliation unknown2
Sahrul WibiyanAffiliation unknown2
Yusuf Mathiinul HakimAffiliation unknown2
Arini Fousty BadriAffiliation unknown2
Patimah Mega Syah Bahar Nur SiregarAffiliation unknown2
Novie JuleantiAffiliation unknown2
NormahAffiliation unknown2
Sherly AgustinaAffiliation unknown1
Elfita ElfitaAffiliation unknown1
Zaqiya Artha ZaharaAffiliation unknown1
Rohmatullaili RohmatullailiAffiliation unknown1
Rahma Dinta AstutiAffiliation unknown1
Aldes Lesbani Aldes LesbaniAffiliation unknown1
Agnes AgnesAffiliation unknown1
Randi O. SaragihAffiliation unknown1
Marieska VerawatyAffiliation unknown1
Suheryanto SuheryantoAffiliation unknown1
Addy RachmatAffiliation unknown1
Bakri Rio RahayuAffiliation unknown1
Rezonsi RezonsiAffiliation unknown1
Fitri Suryani ArsyadAffiliation unknown1
MardiyantoAffiliation unknown1
AmriAffiliation unknown1
ElfitaAffiliation unknown1
Satria Jaya PriatnaAffiliation unknown1
Muhammad Afif AlfariziAffiliation unknown1

Affiliations come from OpenAlex; journal OAI-PMH metadata carries none. Authors without an OpenAlex ID are matched by name, which can merge or split people.

Metadata source: OAI-PMH (metadata jurnal) http://sciencetechindonesia.com/index.php/jsti/oai, first harvested 10 Nov 2026, last seen 10 Nov 2026.
Original metadata (oai_dc) 
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	<dc:title xml:lang="en-US">Preparation, characterization, and thermal stability of B2O3-ZrO2</dc:title>
	<dc:creator>Simbolon, Theresia Debora</dc:creator>
	<dc:creator>Mohadi, Risfidian</dc:creator>
	<dc:description xml:lang="en-US">Synthesis of the borate-based compound with ZrOCl2 to form B2O3-ZrO2 has been conducted. The compound was characterized by FT-IR spectrophotometer, X-ray diffraction, acidity and thermal stability test. The results showed that the FT-IR main vibration spectrum of B2O3-ZrO2 compound has appeared at wave number 401.2 cm-1 for Zr-O bonding vibration, 617.2 cm-1 for B-O-B bonding vibration and 910.4 cm-1 for B-O bonding vibration. The XRD diffraction pattern shows B2O3-ZrO2 compound has an amorphous structure. The FT-IR spectrum after saturated with ammonia and potentiometric titration indicates that the compound of B2O3-ZrO2 has acidic properties with a strong level of acidity. Thermal stability test shows that the B2O3-ZrO2 compounds have high stability on temperature with increasing crystallinity after the compound was heated at 700 °C.
Keywords: B2O3-ZrO2, impregnation, thermal stability. &amp;nbsp;</dc:description>
	<dc:publisher xml:lang="en-US">Research Center of Inorganic Materials and Coordination Complexes, FMIPA Universitas Sriwijaya</dc:publisher>
	<dc:date>2017-04-10</dc:date>
	<dc:type>info:eu-repo/semantics/article</dc:type>
	<dc:type>info:eu-repo/semantics/publishedVersion</dc:type>
	<dc:type xml:lang="en-US">Peer-reviewed Article</dc:type>
	<dc:format>application/pdf</dc:format>
	<dc:identifier>http://sciencetechindonesia.com/index.php/jsti/article/view/20</dc:identifier>
	<dc:identifier>10.26554/sti.2017.2.2.56-58</dc:identifier>
	<dc:source xml:lang="en-US">Science and Technology Indonesia; Vol. 2 No. 2 (2017): April; 56-58</dc:source>
	<dc:source>2580-4391</dc:source>
	<dc:source>2580-4405</dc:source>
	<dc:language>eng</dc:language>
	<dc:relation>http://sciencetechindonesia.com/index.php/jsti/article/view/20/29</dc:relation>
	<dc:rights xml:lang="en-US">Copyright (c) 2017 Science &amp; Technology Indonesia</dc:rights>
</oai_dc:dc>